Department of Chemical and Biochemical Engineering, Dongguk University-Seoul, 04620 Seoul, Korea.
Molecules. 2020 May 13;25(10):2298. doi: 10.3390/molecules25102298.
The present study aimed to explore the eco-friendly synthesis of prism-like silver oxide nanoparticles (AgONPs) from nappa cabbage extract and its -nitrophenol sensing activity. The prepared AgONPs were characterized by X-ray diffraction (XRD), field-emission scanning spectroscopy (FESEM), energy-dispersive spectroscopy (EDS), transmission electron microscopy (TEM), and ultraviolet (UV)-visible light spectral analysis (UV-Vis). -Nitrophenol sensing properties of the prepared nanoparticles were also determined using a simple I-V method. The results showed that the as-prepared AgONPs have a face-centered cubic (fcc) crystalline nature and a prism-like morphology with particle size in the range 21.61-92.26 nm. The result also showed a high intensity of the (111) facet, making the AgONP-carbon black/nickel foam electrode (AgONP-C/NFE) exhibit a high-performance response to -nitrophenol spanning a wide range of concentrations from 1.0 mM to 0.1 pM and a response time of around 5 s, indicating a high potential for water treatment applications.
本研究旨在探索从结球白菜提取物中进行环保型合成氧化银纳米棱柱(AgONPs)及其对-硝基苯酚的传感活性。所制备的 AgONPs 通过 X 射线衍射(XRD)、场发射扫描电子显微镜(FESEM)、能谱(EDS)、透射电子显微镜(TEM)和紫外-可见分光光度计(UV-Vis)进行了表征。使用简单的 I-V 方法确定了所制备的纳米粒子的-硝基苯酚传感性能。结果表明,所制备的 AgONPs 具有面心立方(fcc)晶体性质和棱柱形状,粒径范围为 21.61-92.26nm。结果还显示出(111)面的高强度,使得 AgONP-碳黑/镍泡沫电极(AgONP-C/NFE)对-硝基苯酚表现出宽浓度范围(从 1.0mM 到 0.1pM)的高性能响应,响应时间约为 5s,表明在水处理应用中具有很高的潜力。