Department of Physics, Sree Devi Kumari Women's College, Kuzhithurai 629 163, Tamil Nadu, India.
Department of Physics, Mother Teresa Women's University, Kodaikanal 624101,Tamil Nadu, India.
J Photochem Photobiol B. 2020 Apr;205:111836. doi: 10.1016/j.jphotobiol.2020.111836. Epub 2020 Feb 21.
The present study aimed to explore the biosynthesis and characterization of silver nanoparticles (AgNPs) from Moringa oleifera flower (MOF) extract and its antimicrobial and sensing properties. The prepared AgNPs were characterized by Transmission Electron Microscopy (TEM), UV-visible spectral analysis (UV-vis), X-Ray Diffraction (X-RD), Energy Dispersive Spectroscopy (EDS), and Fourier Infra-Red Spectroscopy (FTIR) respectively. Antimicrobial and sensing properties of the prepared nanoparticles were also determined. Face-Centered Cubic (FCC) lattice of the AgNPs was observed in X-RD pattern. FTIR measurement evidenced the band pattern at 686, 1653, 2062 and 3456 cm proved the presence of proteins and phenolic components in MOF responsible for reduction. TEM analysis indicated the formation of monodispersed spherical particles with 8 nm. UV-vis of the prepared AgNPs authenticated the surface plasmon resonance (SPR) at 429 nm and stable for six months. AgNPs have produced highest zone of inhibition (ZOI) of 17 mm and 29 mm against Klebsiella pneumoniae and Staphylococcus aureus respectively. In addition, the AgNPs effectively detected the presence of Copper ions from 1 mM to 12 mM concentrations. Copper sensitivity of these biosynthesized nanoparticles was carried out by optical sensor based SPR. Thus the obtained antimicrobial and optical properties, suggested the use of obtained AgNPs in water purification.
本研究旨在探索从辣木花(MOF)提取物中生物合成和表征银纳米粒子(AgNPs)及其抗菌和传感性能。通过透射电子显微镜(TEM)、紫外可见光谱分析(UV-vis)、X 射线衍射(X-RD)、能谱(EDS)和傅里叶变换红外光谱(FTIR)分别对制备的 AgNPs 进行了表征。还测定了所制备的纳米粒子的抗菌和传感性能。X-RD 图谱中观察到银纳米粒子的面心立方(FCC)晶格。FTIR 测量证明了在 686、1653、2062 和 3456 cm 处存在蛋白质和酚类成分的带图案,这证明了 MOF 中存在负责还原的蛋白质和酚类成分。TEM 分析表明形成了具有 8nm 的单分散球形颗粒。制备的 AgNPs 的紫外可见光谱证明了表面等离子体共振(SPR)在 429nm 处,并且在六个月内稳定。AgNPs 对肺炎克雷伯菌和金黄色葡萄球菌的抑菌圈(ZOI)分别为 17mm 和 29mm。此外,AgNPs 能够有效地检测从 1mM 到 12mM 浓度的铜离子的存在。这些生物合成的纳米粒子的铜敏感性是通过基于 SPR 的光学传感器进行的。因此,所获得的抗菌和光学性能表明,所获得的 AgNPs 可用于水净化。