Tang Peng, Liu Yiyuan, Zhao Yanjun, Hu Zhiliu, Wang Huachun, Peng Linxin, Deng Songyun, Huang Kui
School of Resources, Environment and Materials, Guangxi University, Nanning, China 530004.
Guangxi Key Laboratory of Processing for Non-ferrous Metal and Featured Materials, Guangxi University, Nanning, China 530004.
Scanning. 2020 Apr 29;2020:9147871. doi: 10.1155/2020/9147871. eCollection 2020.
In this paper, the effect of Er addition (0.2, 0.5, 0.65, 0.8, 1.0, and 1.5 wt. %) on the microstructure evolution and tensile properties of as-cast hypereutectic Al-10Si-0.8Fe alloy was investigated. The phases and their morphologies in these alloys were identified by XRD and SEM equipped with EDX with the help of metallographic analysis techniques; the length of the secondary phase (LSP) and secondary dendrite arm spacing (SDAS) of -Al grain were quantified. The results indicated that the second phases (primary Si, eutectic Si, and iron-rich phases) and -Al grain were significantly refined when the addition of Er increased from 0 to 0.8 wt. %. The mean LSP and SADS values were decreased to a minimum value when the Er addition reached 0.8 wt. %. However, the second phases and -Al grain became coarser when the level of Er increased more than 0.8 wt. %. The analysis of XRD shows that Er mainly exists in the form of ErSi compound. The microstructure modification also has a significant effect on the mechanical properties of the alloy. The yield strength (YS), ultimate tensile strength (UTS), and elongation (EL) increase from 52.86 MPa, 163.84 MPa, and 3.45% to 71.01 MPa, 163.84 MPa, and 5.65%, respectively. From the fracture surface, the promotions of mechanical properties are due to the dispersion and pinning reinforcement caused by the ErSi phase.
本文研究了添加铒(0.2、0.5、0.65、0.8、1.0和1.5 wt.%)对铸态过共晶Al-10Si-0.8Fe合金微观组织演变和拉伸性能的影响。借助金相分析技术,通过配备能谱仪的XRD和SEM对这些合金中的相及其形态进行了鉴定;对α-Al晶粒的二次相长度(LSP)和二次枝晶臂间距(SDAS)进行了量化。结果表明,当铒的添加量从0增加到0.8 wt.%时,第二相(初生硅、共晶硅和富铁相)和α-Al晶粒显著细化。当铒的添加量达到0.8 wt.%时,平均LSP和SADS值降至最小值。然而,当铒含量超过0.8 wt.%时,第二相和α-Al晶粒变得更粗大。XRD分析表明,铒主要以ErSi化合物的形式存在。微观组织的改性对合金的力学性能也有显著影响。屈服强度(YS)、抗拉强度(UTS)和伸长率(EL)分别从52.86 MPa、163.84 MPa和3.45%提高到71.01 MPa、163.84 MPa和5.65%。从断口表面来看,力学性能的提高归因于ErSi相引起的弥散和钉扎强化。