Cosma Cosmin, Drstvensek Igor, Berce Petru, Prunean Simon, Legutko Stanisław, Popa Catalin, Balc Nicolae
Department of Manufacturing Engineering, Technical University of Cluj-Napoca, 400641 Cluj-Napoca, Romania.
Faculty of Mechanical Engineering, University of Maribor, 2000 Maribor, Slovenia.
Materials (Basel). 2020 Sep 16;13(18):4123. doi: 10.3390/ma13184123.
The demand of lattice structures for medical applications is increasing due to their ability to accelerate the osseointegration process, to reduce the implant weight and the stiffness. Selective laser melting (SLM) process offers the possibility to manufacture directly complex lattice applications, but there are a few studies that have focused on biocompatible Ti6Al7Nb alloy. The purpose of this work was to investigate the physical-mechanical properties and the microstructure of three dissimilar lattice structures that were SLM-manufactured by using Ti6Al7Nb powder. In particular, the strut morphology, the fracture characterization, the metallographic structure, and the X-ray phase identification were analyzed. Additionally, the Gibson-Ashby prediction model was adapted for each lattice topology, indicating the theoretical compressive strength and Young modulus. The resulted porosity of these lattice structures was approximately 56%, and the pore size ranged from 0.40 to 0.91 mm. Under quasi-static compression test, three failure modes were recorded. Compared to fully solid specimens, the actual lattice structures reduce the elastic modulus from 104 to 6-28 GPa. The struts surfaces were covered by a large amount of partial melted grains. Some solidification defects were recorded in struts structure. The fractographs revealed a brittle rupture of struts, and their microstructure was mainly α' martensite with columnar grains. The results demonstrate the suitability of manufacturing lattice structures made of Ti6Al7Nb powder having unique physical-mechanical properties which could meet the medical requirements.
由于晶格结构能够加速骨整合过程、减轻植入物重量并降低刚度,其在医学应用中的需求正在不断增加。选择性激光熔化(SLM)工艺为直接制造复杂的晶格应用提供了可能性,但仅有少数研究关注具有生物相容性的Ti6Al7Nb合金。这项工作的目的是研究使用Ti6Al7Nb粉末通过SLM制造的三种不同晶格结构的物理力学性能和微观结构。具体而言,分析了支柱形态、断裂特征、金相组织和X射线相鉴定。此外,针对每种晶格拓扑结构对吉布森-阿什比预测模型进行了调整,以表明理论抗压强度和杨氏模量。这些晶格结构的孔隙率约为56%,孔径范围为0.40至0.91毫米。在准静态压缩试验中,记录到三种失效模式。与完全实心的试样相比,实际的晶格结构将弹性模量从104 GPa降低至6 - 28 GPa。支柱表面覆盖着大量部分熔化的晶粒。在支柱结构中记录到一些凝固缺陷。断口分析显示支柱发生脆性断裂,其微观结构主要是具有柱状晶粒的α'马氏体。结果表明,制造由Ti6Al7Nb粉末制成的具有独特物理力学性能且能满足医学要求的晶格结构是可行的。