Lim Na-Kyung, Shin Soo-Yeon
Department of Prosthodontics, College of Dentistry, Dankook University, Cheonan, Republic of Korea.
J Adv Prosthodont. 2020 Oct;12(5):322-328. doi: 10.4047/jap.2020.12.5.322. Epub 2020 Oct 26.
This study evaluated the shear bond strength between 3D printed provisional resin and conventional provisional resin depending on type of conventional provisional resin and different surface treatments of 3D printed resin.
Ninety-six disc-shaped specimens (Ø14 mm × 20 mm thickness) were printed with resin for 3D printing (Nextdent C&B, Vertex-Dental B. V., Soesterberg, Netherlands). After post-processing, the specimens were randomly divided into 8 groups (n=12) according to two types of conventional repair resin (methylmethacrylate and bis-acryl composite) and four different surface treatments: no additional treatment, air abrasion, soaking in methylmethacrylate (MMA) monomer, and soaking in MMA monomer after air abrasion. After surface treatment, each repair resin was bonded in cylindrical shape using a silicone mold. Specimens were stored in 37℃ distilled water for 24 hours. The shear bond strength was measured using a universal testing machine at a crosshead speed of 0.5 mm/min. Failure modes were analyzed by scanning electron microscope. Statistical analysis was done using one-way ANOVA test and Kruskal-Wallis test (α=.05).
The group repaired with bis-acryl composite without additional surface treatment showed the highest mean shear bond strength. It was significantly higher than all four groups repaired with methylmethacrylate (<.05). Additional surface treatments, neither mechanical nor chemical, increased the shear bond strength within methylmethacrylate groups and bis-acryl composite groups (>.05). Failure mode analysis showed that cohesive failure was most frequent in both methylmethacrylate and bis-acryl composite groups.
Our results suggest that when repairing 3D printed provisional restoration with conventional provisional resin, repair with bis-acryl composite without additional surface treatment is recommended.
本研究根据传统临时树脂的类型和3D打印树脂的不同表面处理方式,评估3D打印临时树脂与传统临时树脂之间的剪切粘结强度。
用3D打印树脂(Nextdent C&B,Vertex-Dental B.V.,荷兰索斯特贝赫)打印96个圆盘形试件(直径14mm×厚度20mm)。后处理后,根据两种传统修复树脂(甲基丙烯酸甲酯和双丙烯酸复合树脂)和四种不同的表面处理方式,将试件随机分为8组(n = 12):不进行额外处理、空气喷砂、浸泡在甲基丙烯酸甲酯(MMA)单体中以及空气喷砂后浸泡在MMA单体中。表面处理后,使用硅胶模具将每种修复树脂粘结成圆柱形。试件在37℃蒸馏水中储存24小时。使用万能试验机以0.5mm/min的十字头速度测量剪切粘结强度。通过扫描电子显微镜分析失效模式。采用单因素方差分析和Kruskal-Wallis检验进行统计分析(α = 0.05)。
未进行额外表面处理的双丙烯酸复合树脂修复组显示出最高的平均剪切粘结强度。它显著高于所有用甲基丙烯酸甲酯修复的四组(P < 0.05)。额外的表面处理,无论是机械处理还是化学处理,在甲基丙烯酸甲酯组和双丙烯酸复合树脂组中均未提高剪切粘结强度(P > 0.05)。失效模式分析表明,甲基丙烯酸甲酯组和双丙烯酸复合树脂组中内聚破坏最为常见。
我们的结果表明,当用传统临时树脂修复3D打印临时修复体时,建议使用未进行额外表面处理的双丙烯酸复合树脂进行修复。