Department of Animal Production, E.T.S.I.A.M., Universidad de Córdoba, Campus Rabanales, 14071, Córdoba, Spain.
Department of Statistical Science, University College London, 1-19 Torrington Place, WC1E 6BT, London, UK.
Talanta. 2021 Jan 15;222:121511. doi: 10.1016/j.talanta.2020.121511. Epub 2020 Aug 13.
Iberian pig ham is one of several high value European food products that are the subject of significant attempts at fraud because of the high price differences between commercial categories. Iberian pig products are classified by the Spanish regulations into different categories, mainly depending on the feeding regime during the fattening phase and the race involved, being of Premium quality those products obtained from the animals fed with acorns and other natural resources. Most of the previous NIRS studies related to the Iberian pig have involved the use of at-line instruments to predict quantitative quality parameters. This paper explores the use of the NIR spectra (369 for training and 199 for validation) to classify samples according to the categories Premium (animals fed with acorn) and Non Premium (animals fed with compound feeds), using a MicroNIR™ Pro1700 microspectrometer to analyse individual carcasses in situ at the slaughterhouse line. Four discriminant methods were explored: linear discriminant analysis (LDA), quadratic discriminant analysis (QDA), Kernel Bayes and Logistic Regression. These are all discriminant methods that naturally produce classification probabilities to quantify the uncertainty of the results. Rules were tuned and methods compared using both classification error rates and a probability scoring rule. LDA gave the best results, attaining an overall accuracy of 93% and providing well-calibrated classification probabilities.
伊比利亚猪火腿是几种高价值的欧洲食品之一,由于商业类别之间存在巨大的价格差异,因此成为了大量欺诈行为的目标。西班牙法规将伊比利亚猪产品分为不同类别,主要取决于育肥阶段的饲养方式和涉及的品种,那些由食用橡子和其他天然资源饲养的动物获得的产品为优质产品。大多数之前与伊比利亚猪相关的 NIRS 研究都涉及使用在线仪器来预测定量质量参数。本文探讨了使用 NIR 光谱(用于训练的 369 个和用于验证的 199 个)根据优质(用橡子喂养的动物)和非优质(用复合饲料喂养的动物)类别对样本进行分类的方法,使用 MicroNIR™ Pro1700 微光谱仪在屠宰场线原位分析单个胴体。探索了四种判别方法:线性判别分析(LDA)、二次判别分析(QDA)、核贝叶斯和逻辑回归。这些都是自然产生分类概率的判别方法,用于量化结果的不确定性。使用分类错误率和概率评分规则调整规则并比较方法。LDA 给出了最佳结果,总体准确率达到 93%,并提供了校准良好的分类概率。