Cubero Álvaro, Martínez Elena, Angurel Luis A, de la Fuente Germán F, Navarro Rafael, Legall Herbert, Krüger Jörg, Bonse Jörn
Instituto de Nanociencia y Materiales de Aragón (INMA), CSIC-Universidad de Zaragoza, 50009 Zaragoza, Spain.
Bundesanstalt für Materialforschung und -prüfung (BAM), Unter den Eichen 87, 12205 Berlin, Germany.
Nanomaterials (Basel). 2020 Dec 16;10(12):2525. doi: 10.3390/nano10122525.
Irradiation with ultra-short (femtosecond) laser beams enables the generation of sub-wavelength laser-induced periodic surface structures (LIPSS) over large areas with controlled spatial periodicity, orientation, and depths affecting only a material layer on the sub-micrometer scale. This study reports on how fs-laser irradiation of commercially available Nb foil samples affects their superconducting behavior. DC magnetization and AC susceptibility measurements at cryogenic temperatures and with magnetic fields of different amplitude and orientation are thus analyzed and reported. This study pays special attention to the surface superconducting layer that persists above the upper critical magnetic field strength , and disappears at a higher nucleation field strength . Characteristic changes were distinguished between the surface properties of the laser-irradiated samples, as compared to the corresponding reference samples (non-irradiated). Clear correlations have been observed between the surface nanostructures and the nucleation field , which depends on the relative orientation of the magnetic field and the surface patterns developed by the laser irradiation.
用超短(飞秒)激光束进行辐照能够在大面积上生成具有可控空间周期性、取向和深度的亚波长激光诱导周期性表面结构(LIPSS),且仅在亚微米尺度上影响材料层。本研究报告了飞秒激光辐照市售铌箔样品如何影响其超导行为。因此,分析并报告了在低温温度下以及不同幅度和取向磁场下的直流磁化强度和交流磁化率测量结果。本研究特别关注在上临界磁场强度以上持续存在且在更高的成核场强度下消失的表面超导层。与相应的参考样品(未辐照)相比,区分了激光辐照样品表面性质的特征变化。已经观察到表面纳米结构与成核场之间存在明显的相关性,成核场取决于磁场的相对取向以及激光辐照形成的表面图案。