Kumthekar Minal Sanjay, Tewary Shivsagar, Sanyal Pronob Kumar
Department of Prosthodontics and Crown and Bridge, School of Dental Sciences, KIMS-DU, Karad, Maharashtra, India.
J Indian Prosthodont Soc. 2020 Oct-Dec;20(4):394-401. doi: 10.4103/jips.jips_85_20. Epub 2020 Oct 8.
The aim of this study is to evaluate the efficacy of new material ultraviolet (UV) light polymerized clear adhesive on shear and tensile bond strength of heat cure denture base resin (Polymethylmethacrylate (PMMA)) to cobalt-chromium (Co-Cr) retentive minor connector.
Comparative evaluation- In-vitro study.
Sixty samples of Co-Cr plates mimicking minor connectors were fabricated. Thirty samples were coated with new material UV light polymerized clear adhesive and cured under UV light source for 10 min. In gun-metal flask, metal plates were placed in the lower compartment over it. Heat cure acrylic resin was packed in the dough stage with the help of clamps and processed according to the manufacturer's instructions. Samples were kept in artificial saliva for 90 days. Shear and tensile bond strengths were calculated of each sample with a Universal testing machine, and results were statistically analyzed. Type of bond failure was observed for each sample under stereomicroscope.
Unpaired t test.
Tensile bond strength, as well as shear bond strength, showed that 0.93 N and 1.64 N respectively for without application of new adhesive was more as compared to that of samples with the application of new adhesive which is 0.75 N and 1.54 N respectively. Bond failure was found to be an adhesive failure in resin-metal interface.
Excellent bonding seen between the new adhesive and acrylic interface but limited effect on the metal interface. To increase bond strength between metal and resin interface, some surface treatment with the metal surface is needed to increase the bonding of the new adhesive to the metal surface.
本研究旨在评估新型紫外线(UV)光固化透明胶粘剂对热固化义齿基托树脂(聚甲基丙烯酸甲酯(PMMA))与钴铬(Co-Cr)固位小连接体的剪切和拉伸粘结强度。
对比评估——体外研究。
制作60个模拟小连接体的Co-Cr板样本。30个样本涂覆新型紫外线光固化透明胶粘剂,并在紫外线光源下固化10分钟。在炮铜铸型中,将金属板置于其下部隔层。在面团期借助夹具填充热固化丙烯酸树脂,并按照制造商说明进行加工。样本在人工唾液中保存90天。用万能试验机计算每个样本的剪切和拉伸粘结强度,并对结果进行统计学分析。在体视显微镜下观察每个样本的粘结失败类型。
非配对t检验。
拉伸粘结强度和剪切粘结强度显示,未使用新型胶粘剂的样本分别为0.93 N和1.64 N,高于使用新型胶粘剂的样本,后者分别为0.75 N和1.54 N。粘结失败为树脂-金属界面的粘结剂破坏。
新型胶粘剂与丙烯酸界面之间粘结良好,但对金属界面的作用有限。为提高金属与树脂界面的粘结强度,需要对金属表面进行一些表面处理,以增强新型胶粘剂与金属表面的粘结。