Graduate Student, Department of Prosthodontics, Graduate School, Chonnam National University, Gwang-Ju, Korea.
J Adv Prosthodont. 2009 Mar;1(1):41-6. doi: 10.4047/jap.2009.1.1.41. Epub 2009 Mar 31.
The poor chemical bonding of a denture base resin to cast titanium framework often introduces adhesive failure and increases microleakage.
This study evaluated the shear bond strengths of a heat cure denture base resin to commercially pure titanium, Ti-6Al-4V alloy and a cobalt-chromium alloy using two adhesive primers.
Disks of commercially pure titanium, Ti-6Al-4V alloy and a cobalt-chromium alloy were cast. Specimens without the primer were also prepared and used as the controls. The shear bond strengths were measured on a screw-driven universal testing machine.
The primers significantly (P < .05) improved the shear bond strengths of the heat cure resin to all metals. However, the specimens primed with the Alloy primer® (MDP monomer) showed higher bond strength than those primed with the MR bond® (MAC-10 monomer) on titanium. Only adhesive failure was observed at the metal-resin interface in the non-primed specimens, while the primed specimens showed mixed failure of adhesive and cohesive failure.
The use of appropriate adhesive metal primers makes it possible not only to eliminate the need for surface preparation of the metal framework before applying the heat cure resins, but also reduce the need for retentive devices on the metal substructure. In particular, the Alloy primer®, which contains the phosphoric acid monomer, MDP, might be clinically more acceptable for bonding a heat cure resin to titanium than a MR bond®, which contains the carboxylic acid monomer, MAC-10.
义齿基托树脂与铸造钛框架之间的化学键结合不良通常会导致粘接力失效并增加微渗漏。
本研究使用两种胶粘剂底漆评估热固性义齿基托树脂与纯钛、Ti-6Al-4V 合金和钴铬合金的剪切结合强度。
铸造纯钛、Ti-6Al-4V 合金和钴铬合金的圆盘。也制备了没有底漆的样品作为对照。在螺旋驱动万能试验机上测量剪切结合强度。
底漆显著(P<.05)提高了热固性树脂对所有金属的剪切结合强度。然而,用 Alloy primer®(MDP 单体)底漆处理的标本在钛上显示出比用 MR bond®(MAC-10 单体)底漆处理的标本更高的结合强度。未底漆处理的标本仅在金属-树脂界面观察到粘接力失效,而底漆处理的标本显示出粘接力和内聚力失效的混合失效。
使用适当的胶粘剂金属底漆不仅可以消除在施加热固性树脂之前对金属框架进行表面处理的需要,还可以减少金属子结构上的固位装置的需要。特别是,含有磷酸单体 MDP 的 Alloy primer®可能比含有羧酸单体 MAC-10 的 MR bond®更适合将热固性树脂粘结到钛上。