Marovic Danijela, Par Matej, Crnadak Ana, Sekelja Andjelina, Negovetic Mandic Visnja, Gamulin Ozren, Rakić Mario, Tarle Zrinka
Department of Endodontics and Restorative Dentistry, School of Dental Medicine, University of Zagreb, Zagreb 10000, Croatia.
Institute for Physics and Biophysics, School of Medicine, University of Zagreb, Zagreb 10000, Croatia.
Materials (Basel). 2021 Jan 21;14(3):515. doi: 10.3390/ma14030515.
This study assessed the influence of rapid 3 s light curing on the new generation of bulk-fill resin composites under the simulated aging challenge and depths up to 4 mm. Four bulk-fill materials were tested: two materials designed for rapid curing (Tetric PowerFill-PFILL; Tetric PowerFlow-PFLW) and two regular materials (Filtek One Bulk Fill Restorative-FIL; SDR Plus Bulk Fill Flowable-SDR). Three-point bending ( = 10) was used to measure flexural strength (FS) and flexural modulus (FM). In the 3 s group, two 2 mm thick specimens were stacked to obtain 4 mm thickness, while 2 mm-thick specimens were used for ISO group. Specimens were aged for 1, 30, or 30 + 3 days in ethanol. The degree of conversion (DC) up to 4 mm was measured by Raman spectroscopy. There was no difference between curing protocols in FS after 1 day for all materials except PFLW. FM was higher for all materials for ISO curing protocol. Mechanical properties deteriorated by increasing depth (2-4 mm) and aging. ISO curing induced higher DC for PFLW and FIL, while 3 s curing was sufficient for PFILL and SDR. The 3 s curing negatively affected FM of all tested materials, whereas its influence on FS and DC was highly material-specific.
本研究评估了在模拟老化挑战以及深度达4毫米的情况下,快速3秒光固化对新一代大体积填充树脂复合材料的影响。测试了四种大体积填充材料:两种专为快速固化设计的材料(Tetric PowerFill - PFILL;Tetric PowerFlow - PFLW)和两种常规材料(Filtek One Bulk Fill Restorative - FIL;SDR Plus Bulk Fill Flowable - SDR)。采用三点弯曲试验(n = 10)来测量弯曲强度(FS)和弯曲模量(FM)。在3秒组中,将两个2毫米厚的试样堆叠以获得4毫米的厚度,而ISO组使用2毫米厚的试样。试样在乙醇中老化1天、30天或30 + 3天。通过拉曼光谱法测量深度达4毫米处的转化率(DC)。除PFLW外,所有材料在老化1天后,固化方案在FS方面无差异。对于所有材料,ISO固化方案的FM更高。机械性能随深度增加(2 - 4毫米)和老化而变差。ISO固化使PFLW和FIL的DC更高,而3秒固化对PFILL和SDR就足够了。3秒固化对所有测试材料的FM有负面影响,而其对FS和DC的影响则具有高度的材料特异性。