Laboratory of Nanostructured Polymers (NANOPOL/@nanopol_ufam), Federal University of Amazonas, Manaus, Amazonas, Brazil.
Federal Institute of Education, Science and Technology of Amazonas, Manaus, Amazonas, Brazil.
Food Res Int. 2021 Jan;139:109838. doi: 10.1016/j.foodres.2020.109838. Epub 2020 Oct 26.
Different carriers, such as the combination of sodium alginate and inulin, have been employed to protect foods against environmental effects. The goal of this work was to use the ionic gelation encapsulation process to produce microparticles containing Clidemia rubra extract, ranging the concentration of inulin from 1.5 to 3.5 g inulin.100 g of solution. Characteristic signals of sugars, organic acids and phenolic compounds were identified in the extract using the H NMR technique. The carriers containing inulin presented significant difference in the moisture content when compared to the pure sodium alginate beads. The produced beads were found in the range of 0.81-1.06 mm. The addition of inulin to sodium alginate was significant for the encapsulation efficiency (EE) of the antioxidant compounds when compared to the beads formed only using pure sodium alginate. The microspheres presenting inulin and sodium alginate presented higher content of spherical particles. The addition of 2.5 g inulin.100 g of solution allowed its incorporation into the pores of the beads, favoring a possible chemical interaction between inulin and sodium alginate. This interaction resulted in a different crystal structure and better EE. Furthermore, beads containing inulin presented higher protection of the encapsulated bioactive compounds during the gastric phase.
不同的载体,如海藻酸钠和菊粉的组合,已被用于保护食品免受环境影响。本工作的目的是使用离子凝胶包埋法生产含 Clidemia rubra 提取物的微球,菊粉浓度为 1.5 至 3.5 g 菊粉。100 g 溶液。采用 H NMR 技术对提取物中的糖、有机酸和酚类化合物的特征信号进行了鉴定。与纯海藻酸钠珠相比,含菊粉的载体在水分含量上有显著差异。所制备的珠粒粒径在 0.81-1.06 mm 之间。与仅使用纯海藻酸钠形成的珠粒相比,菊糖的加入对抗氧化化合物的包封效率(EE)有显著影响。含有菊糖和海藻酸钠的微球具有更高比例的球形颗粒。添加 2.5 g 菊粉。100 g 溶液可将其掺入珠粒的孔隙中,有利于菊糖和海藻酸钠之间可能发生的化学相互作用。这种相互作用导致了不同的晶体结构和更好的 EE。此外,含有菊粉的珠粒在胃阶段对包封生物活性化合物的保护作用更高。