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纳米氧化物粒径对颌面硅橡胶弹性体颜色稳定性和力学性能的影响:一项体外研究。

Effect of Particle Size of Nano-Oxides on Color Stability and Mechanical Properties of Maxillofacial Silicone Elastomers: An In Vitro Study.

出版信息

Int J Prosthodont. 2021 Jan-Feb;34(1):54-60. doi: 10.11607/ijp.6593.

Abstract

PURPOSE

To evaluate the physical and mechanical properties of maxillofacial silicone elastomers following the incorporation of a specific particle size and concentration of nano-titanium dioxide (TiO) and nano-zinc oxide (ZnO).

MATERIALS AND METHODS

Nano-TiO and nano-ZnO of 20-nm and 40-nm particle sizes and in 1% and 2% concentrations were chosen. Silicone elastomer samples were prepared according to the manufacturer's recommendations. The nano-oxides were incorporated via hand spatulation. The samples were subsequently tested for hardness and color stability and were then subjected to aging in an aging chamber for 1,008 hours, following which they were again evaluated for hardness, color stability, and surface roughness.

RESULTS

A significant change was noted in the physical and mechanical properties post-aging in all the groups. The samples with nano-TiO of 40-nm particle size/2% concentration had the highest hardness, while color stability and surface roughness were higher in samples with nano-TiO of 20-nm particle size/1% and 2% concentrations, respectively.

CONCLUSION

It can be concluded that 20-nm nano-TiO particles best maintain the ideal properties of maxillofacial silicone elastomers and can potentially be used as alternative opacifiers when mixed with A-2186 maxillofacial silicone elastomers.

摘要

目的

评估特定粒径和纳米二氧化钛(TiO)和纳米氧化锌(ZnO)浓度的加入对颌面硅橡胶弹性体的物理和机械性能的影响。

材料与方法

选择粒径为 20nm 和 40nm、浓度为 1%和 2%的纳米 TiO 和纳米 ZnO。根据制造商的建议制备硅橡胶弹性体样品。通过手动搓揉将纳米氧化物掺入。随后测试样品的硬度和颜色稳定性,并将其在老化室中老化 1008 小时,然后再次评估硬度、颜色稳定性和表面粗糙度。

结果

所有组在老化后物理和机械性能均发生显著变化。粒径为 40nm、浓度为 2%的纳米 TiO 样品具有最高的硬度,而粒径为 20nm、浓度为 1%和 2%的纳米 TiO 样品的颜色稳定性和表面粗糙度更高。

结论

可以得出结论,20nm 纳米 TiO 颗粒能最佳保持颌面硅橡胶弹性体的理想性能,并在与 A-2186 颌面硅橡胶弹性体混合时可以作为替代不透明剂使用。

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