Go Hye-Bin, Bang Jae-Yun, Kim Kyoung-Nam, Kim Kwang-Mahn, Kwon Jae-Sung
Department and Research Institute of Dental Biomaterials and Bioengineering, Yonsei University College of Dentistry, Seoul 03722, Korea.
BK21 FOUR Project, Yonsei University College of Dentistry, Seoul 03722, Korea.
Materials (Basel). 2021 Feb 9;14(4):827. doi: 10.3390/ma14040827.
The aim of this study was to investigate the element composition and grain size of commercial dental instruments used for ultrasonic scaler tips, which are composed of stainless-steel materials. The differences in mechanical properties and wear resistances were compared. The samples were classified into 4 groups in accordance with the manufacturer, Electro Medical Systems, 3A MEDES, DMETEC and OSUNG MND, and the element compositions of each stainless-steel ultrasonic scaler tip were analyzed with micro-X-ray fluorescence spectrometry (μXRF) and field-emission scanning electron microscopy (FE-SEM) with energy-dispersive X-ray spectroscopy (EDS). One-way ANOVA showed that there were significant differences in shear strength and Vickers hardness among the stainless-steel ultrasonic scaler tips depending on the manufacturer ( < 0.05). The mass before and after wear were found to have no significant difference among groups ( > 0.05), but there was a significant difference in the wear volume loss ( < 0.05). The results were then correlated with μXRF results as well as observations of grain size with optical microscopy, which concluded that the Fe content and the grain size of the stainless steel have significant impacts on strength. Additionally, stainless-steel ultrasonic scaler tips with higher Vickers hardness values showed greater wear resistance, which would be an important wear characteristic for clinicians to check.
本研究的目的是调查由不锈钢材料制成的超声洁牙机工作尖商用牙科器械的元素组成和晶粒尺寸。比较了其机械性能和耐磨性的差异。根据制造商将样本分为4组,分别是Electro Medical Systems、3A MEDES、DMETEC和OSUNG MND,并采用微X射线荧光光谱法(μXRF)以及配备能谱仪(EDS)的场发射扫描电子显微镜(FE-SEM)对每个不锈钢超声洁牙机工作尖的元素组成进行了分析。单因素方差分析表明,不同制造商生产的不锈钢超声洁牙机工作尖在剪切强度和维氏硬度方面存在显著差异(<0.05)。发现各组磨损前后的质量无显著差异(>0.05),但磨损体积损失存在显著差异(<0.05)。然后将结果与μXRF结果以及通过光学显微镜观察的晶粒尺寸相关联,得出不锈钢的铁含量和晶粒尺寸对强度有显著影响的结论。此外,维氏硬度值较高的不锈钢超声洁牙机工作尖显示出更高的耐磨性,这将是临床医生需要检查的一项重要磨损特性。