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化学和机械表面处理对聚醚醚酮与饰面树脂剪切粘结强度影响的比较研究

Comparative Study of Chemical and Mechanical Surface Treatment Effects on The Shear Bond Strength of Polyether-Ether-Ketone to Veneering Resin.

作者信息

Adem Nora, Bal Burcu, Kazazoğlu Ender

出版信息

Int J Prosthodont. 2022 March/April;35(2):201–207. doi: 10.11607/ijp.6938. Epub 2021 Feb 23.

Abstract

PURPOSE

To assess the shear bond strength of composite resin to polyether ether ketone (PEEK) after mechanical and chemical surface treatments.

MATERIALS AND METHODS

A total of 48 PEEK discs were fabricated and divided equally into four surface treatment groups (n = 12 each): (1) airborne particle abrasion with 50-μm alumina particles at 2 MPa pressure for 10 seconds; (2) 98% sulfuric acid etching for 1 minute; (3) airborne particle abrasion and sulfuric acid etching; and (4) no surface treatment. Specimens were conditioned, then Gradia composite veneer (GC) was applied to the PEEK surfaces and polymerized. Bond strength was measured with shear bond test using a universal testing machine. One-way analysis of variance and Tukey post hoc tests were applied for statistical analysis.

RESULTS

The mean shear bond strength values of the sulfuric acid-etched group were higher than that of the airborne particle abrasion + acid etching, airborne particle abrasion, and control groups (P < .05). Mean shear bond strength values for the airborne particle abrasion + acid etching samples were higher than for the control and airborne particle abrasion groups (P < .05).

CONCLUSION

There was no significant difference between the samples treated with airborne particle abrasion and the control group.

摘要

目的

评估在机械和化学表面处理后复合树脂与聚醚醚酮(PEEK)之间的剪切粘结强度。

材料与方法

共制作48个PEEK圆盘,并将其平均分为四个表面处理组(每组n = 12):(1)在2 MPa压力下用50μm氧化铝颗粒进行空气颗粒研磨10秒;(2)用98%硫酸蚀刻1分钟;(3)空气颗粒研磨和硫酸蚀刻;(4)不进行表面处理。对样本进行预处理,然后将Gradia复合贴面(GC)应用于PEEK表面并聚合。使用万能试验机通过剪切粘结试验测量粘结强度。采用单因素方差分析和Tukey事后检验进行统计分析。

结果

硫酸蚀刻组的平均剪切粘结强度值高于空气颗粒研磨+酸蚀刻组、空气颗粒研磨组和对照组(P <.05)。空气颗粒研磨+酸蚀刻样本的平均剪切粘结强度值高于对照组和空气颗粒研磨组(P <.05)。

结论

空气颗粒研磨处理的样本与对照组之间无显著差异。

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