Adem Nora, Bal Burcu, Kazazoğlu Ender
Int J Prosthodont. 2022 March/April;35(2):201–207. doi: 10.11607/ijp.6938. Epub 2021 Feb 23.
To assess the shear bond strength of composite resin to polyether ether ketone (PEEK) after mechanical and chemical surface treatments.
A total of 48 PEEK discs were fabricated and divided equally into four surface treatment groups (n = 12 each): (1) airborne particle abrasion with 50-μm alumina particles at 2 MPa pressure for 10 seconds; (2) 98% sulfuric acid etching for 1 minute; (3) airborne particle abrasion and sulfuric acid etching; and (4) no surface treatment. Specimens were conditioned, then Gradia composite veneer (GC) was applied to the PEEK surfaces and polymerized. Bond strength was measured with shear bond test using a universal testing machine. One-way analysis of variance and Tukey post hoc tests were applied for statistical analysis.
The mean shear bond strength values of the sulfuric acid-etched group were higher than that of the airborne particle abrasion + acid etching, airborne particle abrasion, and control groups (P < .05). Mean shear bond strength values for the airborne particle abrasion + acid etching samples were higher than for the control and airborne particle abrasion groups (P < .05).
There was no significant difference between the samples treated with airborne particle abrasion and the control group.
评估在机械和化学表面处理后复合树脂与聚醚醚酮(PEEK)之间的剪切粘结强度。
共制作48个PEEK圆盘,并将其平均分为四个表面处理组(每组n = 12):(1)在2 MPa压力下用50μm氧化铝颗粒进行空气颗粒研磨10秒;(2)用98%硫酸蚀刻1分钟;(3)空气颗粒研磨和硫酸蚀刻;(4)不进行表面处理。对样本进行预处理,然后将Gradia复合贴面(GC)应用于PEEK表面并聚合。使用万能试验机通过剪切粘结试验测量粘结强度。采用单因素方差分析和Tukey事后检验进行统计分析。
硫酸蚀刻组的平均剪切粘结强度值高于空气颗粒研磨+酸蚀刻组、空气颗粒研磨组和对照组(P <.05)。空气颗粒研磨+酸蚀刻样本的平均剪切粘结强度值高于对照组和空气颗粒研磨组(P <.05)。
空气颗粒研磨处理的样本与对照组之间无显著差异。