Kelić Katarina, Par Matej, Peroš Kristina, Šutej Ivana, Tarle Zrinka
Stomatološka poliklinika Zagreb, Perkovčeva ulica 3, Zagreb, Croatia.
Department of Endodontics and Restorative Dentistry, School of Dental Medicine, University of Zagreb, Gundulićeva 5, Zagreb, Croatia.
Acta Stomatol Croat. 2020 Dec;54(4):371-381. doi: 10.15644/asc54/4/4.
To determine the effect of two adhesive systems and a glass ionomer coating resin on fluoride release and concurrent pH changes over a period of 168 days.
Four restorative materials were investigated: a giomer Beautiful II, an "alkasite" material Cention, a conventional composite Filtek Z250, and a glass ionomer cement Fuji IX Extra. Light-cured composite specimens were coated using G-aenial Bond and Clearfil Universal Bond Quick. Glass ionomer specimens were coated using GC Fuji Coat LC. Uncoated specimens were used as references. Quantitative fluoride release and pH changes were measured after1 h, 24 h, 2 days, 7 days, 28 days, 84 days, and 168 days.
The cumulative fluoride release after 168 days increased for uncoated specimens in the following order: Filtek Z250 < Beautifil II < Cention < Fuji IX Extra. A comparatively lower fluoride release was measured for the composites coated with Clearfil Universal Bond Quick, with cumulative values after 168 days increasing in the following order: Filtek Z250 < Beautifil II < Cention. The composites coated with G-aenial Bond showed lower fluoride release compared to the uncoated specimens, with cumulative values increasing in the following order: Filtek Z250 < Beautifil II < Cention. The composites coated with G-aenial Bond showed pH values in the acidic range (4.4-5.7) after 1 h and 24 h.
Fluoride release varied among the investigated restorative materials and depended on the use of dental adhesives and coatings. The pH of all materials, coating types and time points varied.
确定两种粘结系统和一种玻璃离子涂层树脂在168天内对氟释放及同时发生的pH值变化的影响。
研究了四种修复材料:聚酸改性复合树脂Beautifil II、“碱式玻璃离子”材料Cention、传统复合树脂Filtek Z250和玻璃离子水门汀Fuji IX Extra。光固化复合树脂试件分别用G-aenial Bond和Clearfil Universal Bond Quick进行涂布。玻璃离子试件用GC Fuji Coat LC进行涂布。未涂布的试件用作对照。在1小时、24小时、2天、7天、28天、84天和168天后测量氟的定量释放和pH值变化。
168天后,未涂布试件的累积氟释放量按以下顺序增加:Filtek Z250 < Beautifil II < Cention < Fuji IX Extra。用Clearfil Universal Bond Quick涂布的复合树脂的氟释放量相对较低,168天后的累积值按以下顺序增加:Filtek Z250 < Beautifil II < Cention。用G-aenial Bond涂布的复合树脂与未涂布试件相比氟释放量较低,累积值按以下顺序增加:Filtek Z250 < Beautifil II < Cention。用G-aenial Bond涂布的复合树脂在1小时和24小时后的pH值处于酸性范围(4.4 - 5.7)。
在所研究的修复材料中氟释放量各不相同,且取决于牙科粘结剂和涂层的使用情况。所有材料、涂层类型和时间点的pH值均有所不同。