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用磁控溅射法对阻燃织物涂层质量的评估

Assessment of Coating Quality Obtained on Flame-Retardant Fabrics by a Magnetron Sputtering Method.

作者信息

Miśkiewicz Pamela, Tokarska Magdalena, Frydrych Iwona, Makówka Marcin

机构信息

Faculty of Material Technologies and Textile Design, Institute of Architecture of Textiles, Lodz University of Technology, 116 Zeromskiego St., 90-924 Lodz, Poland.

Faculty of Mechanical Engineering, Institute of Materials Science and Engineering, Lodz University of Technology, 1/15 Stefanowskiego St., 90-924 Lodz, Poland.

出版信息

Materials (Basel). 2021 Mar 11;14(6):1348. doi: 10.3390/ma14061348.

Abstract

Innovative textile materials can be obtained by depositing different coatings. To improve the thermal properties of textiles, aluminum and zirconium (IV) oxides were deposited on the Nomex fabric, basalt fabric, and cotton fabric with flame-retardant finishing using the magnetron sputtering method. An assessment of coating quality was conducted. Evenly coated fabric ensures that there are no places on the sample surface where the values of thermal parameters such as resistance to contact heat and radiant heat deviate significantly from the specified ones. Energy-dispersive spectroscopy was used for the analysis of modified fabric surfaces. Non-contact digital color imaging system DigiEye was also used. The criterion allowing one to compare surfaces and find which surface is more evenly coated was proposed. The best fabrics from the point of view of coating quality were basalt and cotton fabrics coated with aluminum as well as basalt fabric coated with zirconia. The probability of occurrence of places on the indicated sample surfaces where the values of thermal parameters (i.e., resistance to contact heat and radiant heat) deviated significantly from the specified ones was smaller for Nomex and cotton fabrics coated with zirconia and Nomex fabric coated with aluminum.

摘要

通过沉积不同的涂层可以获得创新的纺织材料。为了改善纺织品的热性能,采用磁控溅射法在经过阻燃整理的诺梅克斯织物、玄武岩织物和棉织物上沉积了铝和氧化锆(IV)。对涂层质量进行了评估。涂层均匀的织物可确保样品表面不存在热参数值(如接触热阻和辐射热阻)显著偏离规定值的区域。使用能量色散光谱对改性织物表面进行分析。还使用了非接触式数字彩色成像系统DigiEye。提出了一种用于比较表面并找出哪个表面涂层更均匀的标准。从涂层质量的角度来看,最佳的织物是涂有铝的玄武岩和棉织物以及涂有氧化锆的玄武岩织物。对于涂有氧化锆的诺梅克斯和棉织物以及涂有铝的诺梅克斯织物,在所示样品表面出现热参数值(即接触热阻和辐射热阻)显著偏离规定值的区域的概率较小。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5c57/7998588/9c7ad72ff8f9/materials-14-01348-g001.jpg

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