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硼酸铝晶须增强铝合金复合材料(ABOw/Al-12Si)的高温拉伸蠕变行为

Elevated Temperature Tensile Creep Behavior of Aluminum Borate Whisker-Reinforced Aluminum Alloy Composites (ABOw/Al-12Si).

作者信息

Ji Yameng, Yuan Yanpeng, Zhang Weizheng, Xu Yunqing, Liu Yuwei

机构信息

School of Mechanical Engineering, Beijing Institute of Technology, Beijing 100081, China.

Shandong Binzhou Bohai Piston Co., Ltd., Binzhou 256602, China.

出版信息

Materials (Basel). 2021 Mar 4;14(5):1217. doi: 10.3390/ma14051217.

Abstract

In order to evaluate the elevated temperature creep performance of the ABOw/Al-12Si composite as a prospective piston crown material, the tensile creep behaviors and creep fracture mechanisms have been investigated in the temperatures range from 250 to 400 °C and the stress range from 50 to 230 MPa using a uniaxial tensile creep test. The creep experimental data can be explained by the creep constitutive equation with stress exponents of 4.03-6.02 and an apparent activation energy of 148.75 kJ/mol. The creep resistance of the ABOw/Al-12Si composite is immensely improved by three orders of magnitude, compared with the unreinforced alloy. The analysis of the ABOw/Al-12Si composite creep data revealed that dislocation climb is the main creep deformation mechanism. The values of the threshold stresses are 37.41, 25.85, and 17.36 at elevated temperatures of 300, 350 and 400 °C, respectively. A load transfer model was introduced to interpret the effect of whiskers on the creep rate of this composite. The creep test data are very close to the predicted values of the model. Finally, the fractographs of the specimens were analyzed by Scanning Electron Microscope (SEM), the fracture mechanisms of the composites at different temperatures were investigated. The results showed that the fracture characteristic of the ABOw/Al-12Si composite exhibited a macroscale brittle feature range from 300 to 400 °C, but a microscopically ductile fracture was observed at 400 °C. Additionally, at a low tensile creep temperature (300 °C), the plastic flow capacity of the matrix was poor, and the whisker was easy to crack and fracture. However, during tensile creep at a higher temperature (400 °C), the matrix was so softened that the whiskers were easily pulled out and interfacial debonding appeared.

摘要

为了评估ABOw/Al-12Si复合材料作为一种潜在活塞顶材料的高温蠕变性能,采用单轴拉伸蠕变试验,研究了其在250至400℃温度范围和50至230MPa应力范围内的拉伸蠕变行为及蠕变断裂机制。蠕变实验数据可用应力指数为4.03 - 6.02、表观活化能为148.75kJ/mol的蠕变本构方程来解释。与未增强合金相比,ABOw/Al-12Si复合材料的抗蠕变性能提高了三个数量级。对ABOw/Al-12Si复合材料蠕变数据的分析表明,位错攀移是主要的蠕变变形机制。在300、350和400℃高温下,阈值应力值分别为37.41、25.85和17.36。引入了载荷传递模型来解释晶须对该复合材料蠕变率的影响。蠕变试验数据与模型预测值非常接近。最后,通过扫描电子显微镜(SEM)分析了试样的断口形貌,研究了复合材料在不同温度下的断裂机制。结果表明,ABOw/Al-12Si复合材料的断裂特征在300至400℃范围内呈现宏观脆性特征,但在400℃时观察到微观韧性断裂。此外,在低拉伸蠕变温度(300℃)下,基体的塑性流动能力较差,晶须容易开裂和断裂。然而,在较高温度(400℃)下进行拉伸蠕变时,基体软化,晶须容易被拔出并出现界面脱粘。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/409d/7961456/e97254bb4de3/materials-14-01217-g001.jpg

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