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增材制造不锈钢316L晶格的后处理与表面表征:对生物医学应用的影响

Post-Processing and Surface Characterization of Additively Manufactured Stainless Steel 316L Lattice: Implications for BioMedical Use.

作者信息

Teo Alex Quok An, Yan Lina, Chaudhari Akshay, O'Neill Gavin Kane

机构信息

Department of Orthopaedic Surgery, National University Hospital Singapore, 5 Lower Kent Ridge Road, Singapore 119074, Singapore.

Department of Mechanical Engineering, National University of Singapore, 9 Engineering Drive 1, #07-08 Block EA, Singapore 117575, Singapore.

出版信息

Materials (Basel). 2021 Mar 12;14(6):1376. doi: 10.3390/ma14061376.

Abstract

Additive manufacturing of stainless steel is becoming increasingly accessible, allowing for the customisation of structure and surface characteristics; there is little guidance for the post-processing of these metals. We carried out this study to ascertain the effects of various combinations of post-processing methods on the surface of an additively manufactured stainless steel 316L lattice. We also characterized the nature of residual surface particles found after these processes via energy-dispersive X-ray spectroscopy. Finally, we measured the surface roughness of the post-processing lattices via digital microscopy. The native lattices had a predictably high surface roughness from partially molten particles. Sandblasting effectively removed this but damaged the surface, introducing a peel-off layer, as well as leaving surface residue from the glass beads used. The addition of either abrasive polishing or electropolishing removed the peel-off layer but introduced other surface deficiencies making it more susceptible to corrosion. Finally, when electropolishing was performed after the above processes, there was a significant reduction in residual surface particles. The constitution of the particulate debris as well as the lattice surface roughness following each post-processing method varied, with potential implications for clinical use. The work provides a good base for future development of post-processing methods for additively manufactured stainless steel.

摘要

不锈钢的增材制造越来越容易实现,能够实现结构和表面特性的定制;但对于这些金属的后处理却几乎没有指导。我们开展这项研究,以确定后处理方法的各种组合对增材制造的不锈钢316L晶格表面的影响。我们还通过能量色散X射线光谱法对这些工艺后发现的残留表面颗粒的性质进行了表征。最后,我们通过数字显微镜测量了后处理晶格的表面粗糙度。原生晶格由于部分熔融颗粒而具有可预测的高表面粗糙度。喷砂有效地去除了这一问题,但损坏了表面,引入了一个剥离层,同时还留下了所用玻璃珠的表面残留物。添加研磨抛光或电解抛光去除了剥离层,但引入了其他表面缺陷,使其更易腐蚀。最后,在上述工艺之后进行电解抛光时,残留表面颗粒显著减少。每种后处理方法后的颗粒碎片组成以及晶格表面粗糙度各不相同,对临床应用可能产生影响。这项工作为增材制造不锈钢后处理方法的未来发展提供了良好基础。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b50b/8002108/dcecb3aa55e6/materials-14-01376-g001.jpg

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