Gonzaga Ariane Salgado, Gonzaga David Salgado, Simplício Hallissa, Martins Renato Parsekian, Galvão Marília Regalado, Caldas Sergei Godeiro Fernandes Rabelo
Universidade Federal do Rio Grande do Norte, Departamento de Odontologia (Natal/RN, Brazil).
Universidade Federal do Rio Grande do Norte, Departamento de Engenharia Mecânica (Natal/RN, Brazil).
Dental Press J Orthod. 2021 May 17;26(2):e211945. doi: 10.1590/2177-6709.26.2.e211945.oar. eCollection 2021.
This paper aims to verify the thermodynamic, mechanical and chemical properties of CuNiTi 35ºC commercial wires.
Forty pre-contoured copper-nickel-titanium thermodynamic 0.017 x 0.025-in archwires with an Af temperature of 35°C were used. Eight wires from five different manufacturers (American Orthodontics® [G1], Eurodonto® [G2], Morelli® [G3], Ormco® [G4] and Orthometric® [G5]) underwent cross-sectional dimension measurements, tensile tests, SEM-EDS and differential scanning calorimetry (DSC) tests. Parametric tests (One-way ANOVA and Tukey post-test) were used, with a significance level of 5%, and Pearson's correlation coefficient test was performed between the Af and chemical elements of the wires. All sample tests and statistical analyses were double-blinded.
All wires presented standard dimensions (0.017 x 0.025-in) and superelastic behavior, with mean plateau forces of: G1 = 36.49N; G2 = 27.34N; G3 = 19.24 N; G4 = 37.54 N; and G5 = 17.87N. The Af means were: G1 = 29.40°C, G2 = 29.13°C and G3 = 31.43°C, with p>0.05 relative to each other. G4 (32.77°C) and G5 (35.17°C) presented statistically significant differences between each other and among the other groups. All samples presented Ni, Ti, Cu and Al in different concentrations.
The chemical concentration of the elements that compose the alloy significantly influenced the thermodynamic and mechanical properties.
本文旨在验证35ºC商用铜镍钛丝的热力学、力学和化学性能。
使用40根预成型的0.017×0.025英寸的铜镍钛热力学弓丝,其Af温度为35°C。对来自五个不同制造商(美国正畸公司®[G1]、欧洲齿科公司®[G2]、莫雷利公司®[G3]、奥美科公司®[G4]和正颌测量公司®[G5])的八根弓丝进行横截面尺寸测量、拉伸试验、扫描电子显微镜-能谱分析(SEM-EDS)和差示扫描量热法(DSC)测试。采用参数检验(单因素方差分析和Tukey事后检验),显著性水平为5%,并对弓丝的Af与化学元素之间进行Pearson相关系数检验。所有样本测试和统计分析均采用双盲法。
所有弓丝均呈现标准尺寸(0.017×0.025英寸)和超弹性行为,平均平台力分别为:G1 = 36.49N;G2 = 27.34N;G3 = 19.24N;G4 = 37.54N;G5 = 17.87N。Af的平均值分别为:G1 = 29.40°C,G2 = 29.13°C,G3 = 31.43°C,彼此之间p>0.05。G4(32.77°C)和G5(35.17°C)彼此之间以及与其他组之间存在统计学显著差异。所有样本均呈现不同浓度的镍、钛、铜和铝。
构成合金的元素的化学浓度显著影响热力学和力学性能。