College of Food Science, South China Agricultural University, Guangzhou 510642, China.
College of Food Science, South China Agricultural University, Guangzhou 510642, China; Guangdong Engineering Research Center for Oil-Tea Camellia, Guangzhou 510642, China.
Food Chem. 2021 Dec 1;364:130388. doi: 10.1016/j.foodchem.2021.130388. Epub 2021 Jun 17.
Microwave is a new pretreatment technology, and microwave processing time of camellia seeds is a factor affecting the flavor of camellia seed oil (CSO). Therefore, this study on the characteristic volatile compounds of CSO from microwaved seeds with different processing time was carried out by electronic nose (E-nose), headspace-solid phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-MS) and headspace-gas chromatography-ion mobility spectrometry (HS-GC-IMS). The results of E-nose show that W1W, W2W and W5S were the main sensors to distinguish the flavor profile of CSOs. Through HS-SPME-GC-MS and odor activity value analysis, 80 volatile compounds were detected and 22 key aroma compounds were screened in CSOs. Compared with HS-SPME-GC-MS, 44 volatile compounds were detected by HS-GC-IMS, including 9 identical compounds and 35 different compounds. In general, the volatile compounds of 0, 2 and 3 min CSOs were mainly alcohols and esters, while the 4, 5 and 6 min CSOs were mainly heterocycles and aldehydes.
微波是一种新的预处理技术,微波处理时间是影响茶籽油(CSO)风味的因素之一。因此,本研究采用电子鼻(E-nose)、顶空固相微萃取-气相色谱-质谱联用(HS-SPME-GC-MS)和顶空-气相色谱-离子迁移谱联用(HS-GC-IMS)技术对不同微波处理时间的茶籽制取的 CSO 的特征挥发性化合物进行了研究。E-nose 的结果表明,W1W、W2W 和 W5S 是区分 CSO 风味特征的主要传感器。通过 HS-SPME-GC-MS 和气味活度值分析,在 CSO 中共检测到 80 种挥发性化合物,筛选出 22 种关键香气化合物。与 HS-SPME-GC-MS 相比,HS-GC-IMS 检测到 44 种挥发性化合物,其中 9 种为相同化合物,35 种为不同化合物。总体而言,0、2 和 3 min CSO 的挥发性化合物主要为醇类和酯类,而 4、5 和 6 min CSO 的挥发性化合物主要为杂环和醛类。