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Ti-Si-N纳米复合涂层对防火织物耐热辐射性能的影响

Influence of Ti-Si-N Nanocomposite Coating on Heat Radiation Resistance of Fireproof Fabrics.

作者信息

Miedzińska Danuta, Giełżecki Jan, Mania Ryszard, Marszalek Konstanty, Wolański Robert

机构信息

Faculty of Mechanical Engineering, Military University of Technology, Kaliskiego 2 St., 00-908 Warsaw, Poland.

Faculty of Production and Power Engineering, University of Agriculture in Krakow, 21 Mickiewicza Ave., 30-059 Krakow, Poland.

出版信息

Materials (Basel). 2021 Jun 23;14(13):3493. doi: 10.3390/ma14133493.

DOI:10.3390/ma14133493
PMID:34201605
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8269538/
Abstract

Fireproof fabrics are commonly used for protection of fireguards. Such materials must be characterized by improved heat resistance, especially to radiation and flame. In this paper, fireproof fabric (NATAN and PROTON-trademark names) was covered with Ti-Si-N nanocomposite reflective coating using magnetron sputtering. The fabrics were subjected to heat radiation of heat flux density from 0.615 to 2.525 kW/m. A testing stage equipped with a heat source, thermal imaging camera and thermocouples was used. Two variants of the coatings were studied: Ti-Si and (Ti,Si)N considering different thicknesses of layers. The temperature increment and time to reach the pain threshold (60 °C) which corresponds approximately to a 2nd-degree burn according to Henriques criterion were analyzed. In addition, the microstructural analysis of the samples using a scanning electron microscope (SEM) equipped with energy dispersive spectroscopy (EDS) system was performed. The improvement of heat resistance showed for Ti-Si-coated PROTON and NATAN for all tested heat flux densities. Time to reach 60 °C for PROTON fabric increased maximally from 11.23 s (without coating) to 13.13 s (Ti-Si coating) for heat flux density of 0.615 kW/m and for NATAN-maximally from 7.76 s (without coating) to 11.30 s (Ti-Si coating) for the same heat flux density.

摘要

防火织物通常用于保护消防员。这类材料必须具备更高的耐热性，尤其是对辐射和火焰的耐热性。本文采用磁控溅射法在防火织物（NATAN和PROTON为商标名）上覆盖Ti-Si-N纳米复合反射涂层。对织物施加热流密度为0.615至2.525 kW/m的热辐射。使用了一个配备热源、热成像相机和热电偶的测试平台。研究了两种涂层变体：Ti-Si和(Ti,Si)N，并考虑了不同的层厚度。分析了温度增量以及达到疼痛阈值（60°C，根据亨里克斯标准，该温度大致对应二度烧伤）所需的时间。此外，还使用配备能量色散光谱（EDS）系统的扫描电子显微镜（SEM）对样品进行了微观结构分析。对于所有测试的热流密度，Ti-Si涂层的PROTON和NATAN织物的耐热性均有提高。对于热流密度为0.615 kW/m的情况，PROTON织物达到60°C的时间从（无涂层时的）11.23秒最大增加到（Ti-Si涂层时的）13.13秒，对于NATAN织物，在相同热流密度下，达到60°C的时间从（无涂层时的）7.76秒最大增加到（Ti-Si涂层时的）11.30秒。

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