de Paiva Pablo Henrique Eduardo Nazario, Correa Luana Gabrielle, Paulo Ana Flávia Sampaio, Balan Geane Cristiane, Ida Elza Iouko, Shirai Marianne Ayumi
Coordenação de Engenharia Química (COENQ), Universidade Tecnológica Federal do Paraná, Campus Londrina, Avenida dos Pioneiros, 3131, Londrina, Paraná CEP 86036-370 Brazil.
Departamento Acadêmico de Alimentos (DAALM), Universidade Tecnológica Federal do Paraná, Campus Londrina, Avenida dos Pioneiros, 3131, Londrina, Paraná CEP 86036-370 Brazil.
J Food Sci Technol. 2021 Aug;58(8):3030-3038. doi: 10.1007/s13197-020-04806-7. Epub 2020 Oct 3.
Flaxseed mucilage was extracted with distilled water, dried and used for film production with polyvinyl alcohol (PVA) (ratio 1:1) of different hydrolysis degrees (88.0 and 98.3%). The properties of the films were evaluated by determining the thickness, tensile measurements, moisture content, water vapor permeability, apparent opacity, scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR) analysis and thermogravimetric analysis. Flaxseed mucilage, when mixed with PVA, produces less resistant, less rigid, more-flexible films, has a higher thermal stability, and does not change the water vapor barrier properties compared with pure mucilage films. SEM revealed that films with mucilage and PVA mixtures formed a compact and homogeneous structure, corroborating the FTIR spectra that indicated a chemical interaction between these two biopolymers. In general, the degree of PVA hydrolysis did not influence the properties of the films when mixed with flaxseed mucilage extract. Therefore, films obtained from mixtures of flaxseed mucilage and PVA can be an interesting and advantageous alternative for producing bio-based packaging.
用蒸馏水提取亚麻籽黏液,干燥后与不同水解度(88.0%和98.3%)的聚乙烯醇(PVA)(比例1:1)一起用于制膜。通过测定膜的厚度、拉伸性能、水分含量、水蒸气透过率、表观不透明度、扫描电子显微镜(SEM)、傅里叶变换红外光谱(FTIR)分析和热重分析来评估膜的性能。与纯黏液膜相比,亚麻籽黏液与PVA混合时,制得的膜抗性更小、刚性更低、更柔韧,具有更高的热稳定性,且不改变水蒸气阻隔性能。扫描电子显微镜显示,含有黏液和PVA混合物的膜形成了致密且均匀的结构,这与傅里叶变换红外光谱表明这两种生物聚合物之间存在化学相互作用的结果相符。总体而言,PVA的水解度在与亚麻籽黏液提取物混合时不会影响膜的性能。因此,由亚麻籽黏液和PVA混合物制得的膜可能是生产生物基包装的一种有趣且具有优势的替代选择。