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固相微萃取-气相色谱-质谱联用红外和拉曼技术在蜂蜜植物来源及产地鉴别与掺假检测中的应用

The Use of SPME-GC-MS IR and Raman Techniques for Botanical and Geographical Authentication and Detection of Adulteration of Honey.

作者信息

Sotiropoulou Nefeli Sofia, Xagoraris Marinos, Revelou Panagiota Kyriaki, Kaparakou Eleftheria, Kanakis Charalabos, Pappas Christos, Tarantilis Petros

机构信息

Laboratory of Chemistry, Department of Food Science and Human Nutrition, School of Food and Nutrition Sciences, Agricultural University of Athens, Iera Odos 75, 11855 Athens, Greece.

出版信息

Foods. 2021 Jul 20;10(7):1671. doi: 10.3390/foods10071671.

Abstract

The aim of this review is to describe the chromatographic, spectrometric, and spectroscopic techniques applied to honey for the determination of botanical and geographical origin and detection of adulteration. Based on the volatile profile of honey and using Solid Phase microextraction-Gas chromatography-Mass spectrometry (SPME-GC-MS) analytical technique, botanical and geographical characterization of honey can be successfully determined. In addition, the use of vibrational spectroscopic techniques, in particular, infrared (IR) and Raman spectroscopy, are discussed as a tool for the detection of honey adulteration and verification of its botanical and geographical origin. Manipulation of the obtained data regarding all the above-mentioned techniques was performed using chemometric analysis. This article reviews the literature between 2007 and 2020.

摘要

本综述的目的是描述用于蜂蜜的色谱、光谱和波谱技术,以确定其植物来源和地理来源,并检测掺假情况。基于蜂蜜的挥发性成分,并使用固相微萃取-气相色谱-质谱联用(SPME-GC-MS)分析技术,可以成功确定蜂蜜的植物来源和地理特征。此外,还讨论了使用振动光谱技术,特别是红外(IR)光谱和拉曼光谱,作为检测蜂蜜掺假以及验证其植物来源和地理来源的工具。使用化学计量分析对通过上述所有技术获得的数据进行处理。本文综述了2007年至2020年的文献。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/55e0/8303172/058eb6e16b9c/foods-10-01671-g001.jpg

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