Rahayuningsih Edia, Setiawan Felix Arie, Rahman Ahmad Badawi Kasyfur, Siahaan Tomimoto, Petrus Himawan Tri Bayu Murti
Department of Chemical Engineering, Universitas Gadjah Mada, Jalan Grafika No. 2 Kampus UGM, Yogyakarta, 55281 Indonesia.
Department of Chemical Engineering, Universitas Jember, Jalan Kalimantan No. 37 Kampus Tegalboto, East Java, 68121 Indonesia.
J Food Sci Technol. 2021 Sep;58(9):3379-3387. doi: 10.1007/s13197-020-04910-8. Epub 2020 Nov 20.
Betacyanin is a red natural dye pigment widely used in food products. However, the pigment is also unstable and easily degraded by temperature during storage and food processing. This research aims to increase the stability of betacyanin obtained from dragon fruit peels using pectin as a wall medium via the coacervation method. Due to the efficiency and shell integrity, the coacervation method was selected instead of spray drying to enhance betacyanin's stability. Coacervation was conducted in a three-necked round-bottomed flask fitted with a mercury-sealed stirrer and reflux condenser. An accelerated stability test was conducted at 80 °C and 100 °C for 30 min and considered completed after obtaining a stable absorbance. Two full factorials, three-level design, for 80 °C and 100 °C, were analyzed by Response Surface Methodology using Minitab® 19. The core/wall ratio, agitation speed, and pH were the continuous variables, with temperature as the categorical variables. The models were yielded high R-square and low coefficient of variance on the validation process. Simple coacervation is selected because of a superior method such as simplicity, low-cost, high efficiency, and high shell integrity.
甜菜色素是一种广泛应用于食品中的红色天然染料色素。然而,这种色素也不稳定,在储存和食品加工过程中容易因温度而降解。本研究旨在通过凝聚法,以果胶作为壁材介质,提高从火龙果果皮中提取的甜菜色素的稳定性。由于凝聚法的效率和壳的完整性,选择凝聚法而非喷雾干燥法来提高甜菜色素的稳定性。凝聚过程在装有汞封搅拌器和回流冷凝器的三颈圆底烧瓶中进行。在80℃和100℃下进行30分钟的加速稳定性试验,在获得稳定吸光度后视为完成。使用Minitab® 19通过响应面法对80℃和100℃的两个全因子、三级设计进行分析。核/壁比、搅拌速度和pH值为连续变量,温度为分类变量。这些模型在验证过程中具有较高的决定系数R²和较低的变异系数。选择简单凝聚法是因为它具有诸如简单、低成本、高效率和高壳完整性等优点。