Watts R R, Cupitt L T
U.S. Environmental Protection Agency, Health Effects Research Laboratory, Research Triangle Park, NC 27711.
J Assoc Off Anal Chem. 1987 Nov-Dec;70(6):1069-72.
A sample accountability quality assurance (QA) program is described for a field and laboratory research effort which resulted in collection of approximately 2000 samples for analysis by several EPA and contractor laboratories. A QA program was specifically developed for this research program to include sample transfer from collection site to storage maintenance, record development, transfer to researchers, and sample tracking at all stages. A sample identification system and sample custody records are described for field and laboratory application. The functions of a sample coordinator are also described as relating to sample custody, coordination of sample analysis with researchers, and development of computer record files to facilitate research and sample tracking.
本文描述了一个针对野外和实验室研究工作的样本责任质量保证(QA)计划,该研究共采集了约2000个样本,由多个美国环境保护局(EPA)和承包商实验室进行分析。专门为该研究计划制定了一个QA计划,内容包括从采集地点到储存维护的样本转移、记录建立、样本转移给研究人员以及各阶段的样本追踪。还介绍了适用于野外和实验室的样本识别系统及样本保管记录。文中还阐述了样本协调员的职责,包括样本保管、与研究人员协调样本分析以及建立计算机记录文件以促进研究和样本追踪。