Brykov Michail Nikolaevich, Akrytova Taisiia Oleksandrivna, Osipov Michail Jurievich, Petryshynets Ivan, Puchy Viktor, Efremenko Vasily Georgievich, Shimizu Kazumichi, Kunert Maik, Hesse Olaf
Welding Department, Zaporizhzhia Polytechnic National University, Zhukovsky 64, 69063 Zaporizhzhia, Ukraine.
Division of Metallic Systems, Institute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Kosice, Slovakia.
Materials (Basel). 2021 Oct 17;14(20):6159. doi: 10.3390/ma14206159.
A high-carbon, high-silicon steel (1.21 wt% C, 2.56 wt% Mn, 1.59 wt% Si) was subjected to quenching from 900 and 1000 °C, resulting in microstructures containing 60 and 94% of retained austenite, respectively. Subsequent abrasive wear tests of quenched samples were performed using two-body abrasion and three-body abrasion testing machines. Investigations on worn surface and subsurface were carried out using SEM, XRD, and microhardness measurement. It was found that the highest microhardness of worn surface (about 1400 HV0.05) was achieved on samples quenched from 900 °C after three-body abrasion. Microhardness of samples after two-body abrasion was noticeably smaller. with a maximum of about 1200 HV0.05. This difference correlates with microstructure investigations along with XRD results. Three-body abrasion has produced a significantly deeper deformed layer; corresponding diffractograms show bigger values of the full width at half maximum parameter (FWHM) for both α and γ alone standing peaks. The obtained results are discussed in the light of possible differences in abrasive wear conditions and differing stability of retained austenite after quenching from different temperatures. It is shown that a structure of metastable austenite may be used as a detector for wear conditions, as the sensitivity of such austenite to phase transformation strongly depends on wear conditions, and even small changes in the latter lead to significant differences in the properties of the worn surface.
一种高碳高硅钢(碳含量为1.21 wt%,锰含量为2.56 wt%,硅含量为1.59 wt%)在900℃和1000℃下进行淬火,分别得到残余奥氏体含量为60%和94%的微观组织。随后,使用两体磨损试验机和三体磨损试验机对淬火后的样品进行了磨料磨损试验。利用扫描电子显微镜(SEM)、X射线衍射仪(XRD)和显微硬度测量对磨损表面和次表面进行了研究。结果发现,三体磨损后,900℃淬火的样品磨损表面的显微硬度最高(约1400 HV0.05)。两体磨损后样品的显微硬度明显较小,最大值约为1200 HV0.05。这种差异与微观结构研究以及XRD结果相关。三体磨损产生了明显更深的变形层;相应的衍射图谱显示,单独的α相和γ相的半高宽(FWHM)参数值更大。根据磨料磨损条件的可能差异以及不同温度淬火后残余奥氏体的不同稳定性,对所得结果进行了讨论。结果表明,亚稳奥氏体结构可作为磨损条件的探测器,因为这种奥氏体的相变敏感性强烈依赖于磨损条件,即使后者的微小变化也会导致磨损表面性能的显著差异。