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用于直接桩核构建的新型空心套筒复合材料的评估

Evaluation of New Hollow Sleeve Composites for Direct Post-Core Construction.

作者信息

Yoshii Shinji, Garoushi Sufyan, Kitamura Chiaki, Vallittu Pekka K, Lassila Lippo V

机构信息

Department of Biomaterials Science and Turku Clinical Biomaterial Center-TCBC, Institute of Dentistry, University of Turku, 20500 Turku, Finland.

Division of Promoting Learning Design Education, Kyushu Dental University, Fukuoka 803-8580, Japan.

出版信息

Materials (Basel). 2021 Dec 2;14(23):7397. doi: 10.3390/ma14237397.

Abstract

The preset shape and diameter of a prefabricated FRC post rarely follows the anatomy of the root canal. To solve this problem, a new hollow sleeve composite (HSC) system for post-core construction was developed and characterized. A woven fiber was impregnated with two types of resins: Bis-GMA or PMMA, and rolled into cylinders with outer diameter of 2 mm and two different inner diameters, namely 1.2 or 1.5 mm. The commercial i-TFC system was used as a control. Dual-cure resin composite was injected into these sleeves. Additionally, conventional solid fiber post was used as the inner part of the sleeve. The three-point bending test was used to measure the mechanical properties of the specimens and the fracture surface was examined using an electron microscope (SEM). The HSC (1.5 mm, Bis-GMA) revealed a statistically similar flexural modulus but higher flexural strength (437 MPa) compared to i-TFC (239 MPa; ANOVA, < 0.05). When a fiber post was added inside, all values had a tendency to increase. After hydrothermal accelerated aging, the majority of specimens showed a significant ( < 0.05) decrease in flexural strength and modulus. SEM fracture analysis confirmed that the delamination occurred at the interface between the outer and inner materials. The HSC system provided flexibility but still high mechanical values compared to the commercial system. Thus, this system might offer an alternative practical option for direct post-core construction.

摘要

预制纤维增强复合树脂桩的预设形状和直径很少能与根管解剖结构相符。为解决这一问题,研发并表征了一种用于桩核构建的新型中空套筒复合材料(HSC)系统。将编织纤维浸渍两种树脂:双酚A缩水甘油醚甲基丙烯酸酯(Bis-GMA)或聚甲基丙烯酸甲酯(PMMA),然后卷制成外径为2mm、两种不同内径(即1.2mm或1.5mm)的圆柱体。将市售的i-TFC系统用作对照。将双固化树脂复合材料注入这些套筒中。此外,使用传统的实心纤维桩作为套筒的内部部件。采用三点弯曲试验测量试件的力学性能,并使用电子显微镜(SEM)检查断裂表面。与i-TFC(239MPa;方差分析,P<0.05)相比,HSC(1.5mm,Bis-GMA)的弯曲模量在统计学上相似,但弯曲强度更高(437MPa)。当在内部添加纤维桩时,所有数值都有增加的趋势。水热加速老化后,大多数试件的弯曲强度和模量显著降低(P<0.05)。SEM断裂分析证实,分层发生在外层和内层材料之间的界面处。与市售系统相比,HSC系统具有灵活性,但仍具有较高的力学性能值。因此,该系统可能为直接桩核构建提供一种实用的替代方案。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/51a0/8658817/70a2208e9633/materials-14-07397-g001.jpg

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