Department of Experimental Dentistry, Wroclaw Medical University, 50-425 Wroclaw, Poland.
Department of Conservative Dentistry, Wroclaw Medical University, 50-425 Wroclaw, Poland.
Int J Mol Sci. 2022 Jan 11;23(2):745. doi: 10.3390/ijms23020745.
The aim of the study was to evaluate the influence of thermocycling on the shear bond strength of self-adhesive, self-etching resin cements luted to human dentin and computer-aided design/computer-aided manufacturing (CAD/CAM) ceramics. Three modern self-adhesive dental cements (Maxcem Elite, RelyX U200, Panavia SA) were used to lute three CAD/CAM ceramics (IPS Empress CAD, IPS e.max CAD, IPS e.max ZirCAD) onto the dentin. One conventional cement (Panavia V5) served as a control. After preparation, the samples were subjected to thermocycling as a method of artificial aging of dental materials applied to simulate long-term use in oral conditions. Shear bond strength was evaluated according to PN-EN ISO 29022:2013-10 and failure modes were observed under a light microscope. Statistical analysis was performed. The study demonstrated that a combination of ceramics and cements directly impacts the bond strength. The highest bond strength was observed in Panavia V5, lower in Panavia SA and Maxcem Elite and the lowest-in RelyX U200. Adhesive failure between human dentin and cements was the most common failure mode. Moreover, thermocycling highly decreased bond strength of self-adhesive, self-etching cements.
本研究旨在评估热循环对自粘结、自酸蚀树脂粘结剂粘结于牙本质和计算机辅助设计/计算机辅助制造(CAD/CAM)陶瓷的剪切粘结强度的影响。使用三种现代自粘结牙科粘结剂(Maxcem Elite、RelyX U200、Panavia SA)将三种 CAD/CAM 陶瓷(IPS Empress CAD、IPS e.max CAD、IPS e.max ZirCAD)粘结到牙本质上。一种传统粘结剂(Panavia V5)作为对照。准备后,样品进行热循环,作为模拟长期口腔使用条件下的牙科材料人工老化的方法。根据 PN-EN ISO 29022:2013-10 评估剪切粘结强度,并在光显微镜下观察失效模式。进行了统计分析。研究表明,陶瓷和粘结剂的组合直接影响粘结强度。Panavia V5 的粘结强度最高,Panavia SA 和 Maxcem Elite 的粘结强度较低,而 RelyX U200 的粘结强度最低。牙本质和粘结剂之间的粘结失效是最常见的失效模式。此外,热循环极大地降低了自粘结、自酸蚀粘结剂的粘结强度。