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热加工参数对热变形Zr-45Ti-5Al-3V合金微观组织和织构演变的影响

Effect of Hot Working Parameters on Microstructure and Texture Evolution of Hot-Deformed Zr-45Ti-5Al-3V Alloy.

作者信息

Lei Yuanyuan, Yang Ya, Tan Yuanbiao, Zhang Wenwei, Wu Shanshan, Ma Min

机构信息

Guizhou Key Laboratory of Materials Mechanical Behavior and Microstructure, College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China.

College of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201, China.

出版信息

Materials (Basel). 2022 Feb 13;15(4):1382. doi: 10.3390/ma15041382.

Abstract

The effect of hot working parameters on the microstructure and texture evolution of the hot-deformed Zr-45Ti-5Al-3V alloy was studied by the electron backscatter diffraction (EBSD) technique. It was found that a high density of dislocations were generated when the alloy was deformed at 700 °C/0.001 s and 800 °C/1 s. With the increment in hot-deformation temperature and the decrease in strain rate, the dislocation density decreased due to the increase in dynamic recrystallization (DRX) degree. The discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) mechanisms co-existed during the hot working of the Zr-45Ti-5Al-3V alloy at a true strain of 0.7. The texture evolution of the alloy during hot working was characterized and the texture component mainly consisted of {001}<100>, {011}<100>, {110}<112>, and {112}<110> textures. The volume fractions of {001}<100> and {011}<100> textures obviously rose with the reduction in strain rate, whereas those of {110}<112> and {112}<110> textures gradually decreased. At a given strain rate, an increase trend in the volume fraction of the {001}<100> texture was observed with rising hot-deformation temperature, while the volume fraction of the {011}<100> texture first increased and then decreased. An opposite trend was visible in the {112}<110> and {110}<112> texture compared with {011}<100> textures.

摘要

采用电子背散射衍射(EBSD)技术研究了热加工参数对热变形Zr-45Ti-5Al-3V合金微观组织和织构演变的影响。研究发现,该合金在700℃/0.001 s和800℃/1 s变形时会产生高密度位错。随着热变形温度的升高和应变速率的降低,由于动态再结晶(DRX)程度的增加,位错密度降低。在Zr-45Ti-5Al-3V合金真应变0.7的热加工过程中,不连续动态再结晶(DDRX)和连续动态再结晶(CDRX)机制共存。对合金热加工过程中的织构演变进行了表征,织构组分主要由{001}<100>、{011}<100>、{110}<112>和{112}<110>织构组成。随着应变速率的降低,{001}<100>和{011}<100>织构的体积分数明显升高,而{110}<112>和{112}<110>织构的体积分数逐渐降低。在给定应变速率下,随着热变形温度的升高,{001}<100>织构的体积分数呈增加趋势,而{011}<100>织构的体积分数先增加后降低。与{011}<100>织构相比,{112}<110>和{110}<112>织构呈现相反的趋势。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1f12/8880190/07e68620b876/materials-15-01382-g001.jpg

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