You Jing, Huang Yingjie, Liu Chuming, Zhan Hongyi, Huang Lixin, Zeng Guang
School of Materials Science and Engineering, Central South University, Changsha 410083, China.
China Science Lab, General Motors Global Research and Development, Shanghai 201206, China.
Materials (Basel). 2020 May 20;13(10):2348. doi: 10.3390/ma13102348.
Understanding the correlation of plasticity with deformation and dynamic recrystallization (DRX) behaviors, in magnesium (Mg) alloys deformed under high-strain-rate conditions, is increasingly important for wrought Mg processing. In the present study, a ZK30 (Mg-2.61%Zn-0.66%Zr by weight percent (wt.%)) alloy in the as-forged state was hot compressed to various strain levels at a temperature of 350 °C and a strain rate of 10 s. Heterogeneous deformation and dynamic recrystallization (DRX) behaviors of the complicated microstructures in the deformed samples were analyzed via a grain-partitioning approach based on intra-grain misorientation analysis from electron back-scattered diffraction (EBSD). The ZK30 alloy showed excellent formability, remaining intact at a true strain of -1.11. Continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) via grain boundary corrugation/bulging are the dominant mechanisms for the relaxation of strain energy during hot compression. Initial Zr-rich coarse grains undertook a significant portion of the plastic strain as the compression progressed, reflected by the increased misorientations within their interior and marked change in their aspect ratios. The results indicate that the excellent plasticity of the as-forged ZK30 alloy can be attributed to the operative CDRX mechanisms and the reduced deformation anisotropy of Zr-rich coarse grains containing Zn-Zr nano-precipitates.
了解在高应变速率条件下变形的镁(Mg)合金中,塑性与变形及动态再结晶(DRX)行为之间的相关性,对于变形镁加工而言愈发重要。在本研究中,将锻造态的ZK30(重量百分比(wt.%)为Mg-2.61%Zn-0.66%Zr)合金在350°C温度和10 s-1的应变速率下热压缩至不同应变水平。通过基于电子背散射衍射(EBSD)晶内取向差分析的晶粒划分方法,分析了变形样品中复杂微观结构的非均匀变形和动态再结晶(DRX)行为。ZK30合金表现出优异的可锻性,在真应变达到-1.11时仍保持完整。通过晶界波纹/鼓胀进行的连续动态再结晶(CDRX)和不连续动态再结晶(DDRX)是热压缩过程中应变能释放的主要机制。随着压缩过程的进行,初始富含Zr的粗晶粒承担了很大一部分塑性应变,这体现在其内部取向差的增加以及纵横比的显著变化上。结果表明,锻造态ZK30合金优异的塑性可归因于起作用的CDRX机制以及含Zn-Zr纳米析出相的富含Zr粗晶粒变形各向异性的降低。