J Adhes Dent. 2022 Mar 1;24:49-56. doi: 10.3290/j.jad.b2701705.
To evaluate the influence of dimethyl sulfoxide (DMSO) solutions used as dentin pretreatments on microtensile bond strength (µTBS), as well as the dentin/restoration interface micromorphology of a universal adhesive in etch-and-rinse or self-etch mode.
Eighty blocks of dentin were submitted to acid conditioning with 35% phosphoric acid (etch-and-rinse), or not (self-etch), and distributed among the treatments (n = 10): CON: Scotchbond Universal/3M Oral Care; DMSO: pretreatment with DMSO; DMSO/water: pretreatment with DMSO in water (1:1); DMSO/ethanol: pretreatment with DMSO in ethanol (1:1). Microtensile bond strength and failure tests were performed after 24-h and 6-month storage. The tooth-restoration interface was evaluated using scanning electron microscopy to assess the hybrid layer formed.
The interaction between treatments, storage time, and etching modes was not significant for µTBS (p = 0.2469). The DMSO, DMSO/water and DMSO/ethanol pretreatments did not affect µTBS values at either time point (p = 0.8732). Aging decreased µTBS over time only for the etch-and-rinse strategy, although the groups presented higher microtensile bond strengths in etch-and-rinse mode than in self-etch mode at both time points (p < 0.0001). The micromorphological images of the interface showed that different DMSO pretreatment solutions did not impair hybrid layer formation.
The use of dentin pretreatments containing DMSO did not improve the bonding or the micromorphology of a universal adhesive in etch-and-rinse or self-etch modes.
评估二甲基亚砜(DMSO)溶液作为牙本质预处理对通用粘结剂微拉伸粘结强度(µTBS)的影响,以及酸蚀-冲洗或自酸蚀模式下通用粘结剂在牙本质/修复体界面的微观形态。
80 个牙本质块接受 35%磷酸酸蚀(酸蚀-冲洗)或不酸蚀(自酸蚀)处理,并分为以下处理组(n=10):CON: Scotchbond Universal/3M Oral Care;DMSO:DMSO 预处理;DMSO/水:DMSO 与水(1:1)混合预处理;DMSO/乙醇:DMSO 与乙醇(1:1)混合预处理。24 小时和 6 个月储存后进行微拉伸粘结强度和失效测试。使用扫描电子显微镜评估牙-修复体界面,以评估形成的混合层。
处理、储存时间和蚀刻模式之间的相互作用对µTBS 没有显著影响(p=0.2469)。DMSO、DMSO/水和 DMSO/乙醇预处理在两个时间点均未影响µTBS 值(p=0.8732)。只有在酸蚀-冲洗策略下,随着时间的推移,老化会降低µTBS,但在两个时间点,各组在酸蚀-冲洗模式下的微拉伸粘结强度均高于自酸蚀模式(p<0.0001)。界面的微观形态图像显示,不同的 DMSO 预处理溶液不会损害混合层的形成。
使用含有 DMSO 的牙本质预处理剂并不能改善通用粘结剂在酸蚀-冲洗或自酸蚀模式下的粘结性能或微观形态。