Tayal Anshul, Niyogi Abhijit, Adhikari Haridas Das, Adhya Pampa, Ghosh Amrita
Department of Conservative Dentistry and Endodontics, Dr. R. Ahmed Dental College and Hospital, Kolkata, West Bengal, India.
J Conserv Dent. 2021 Jul-Aug;24(4):336-340. doi: 10.4103/jcd.jcd_293_21. Epub 2022 Jan 13.
Success of all-ceramic restorations depends on their cementation process. Bonding crystalline materials like zirconia to an underlying substrate is challenging. Recently, universal adhesives have been developed. They claim to chemically bond to zirconia due to the presence of compounds like 10-methacryloyloxydecyl dihydrogen phosphate. But for majority of these adhesives, few studies demonstrating their effectiveness are available.
This study aimed to assess the effect of two universal adhesives, One Coat 7 Universal and Tetric N-Bond Universal on shear bond strength at zirconia-resin junction.
Thirty CAD-CAM milled zirconia cylinders (5 mm × 8 mm) were sandblasted and divided into three groups: Group A (control) received no treatment, while Groups B and C were primed by One Coat 7 Universal and Tetric N-Bond Universal, respectively. They were luted to composite surfaces by a dual-curing resin cement. After 24 h, a shear bond strength test was conducted and failure mode was analyzed.
One-way analysis of variance and Tukey's test were used for statistical analysis.
Both One Coat 7 Universal (24.43 ± 2.66 MPa) and Tetric N-Bond Universal (28.61 ± 3.11 MPa) had significantly higher strength than the control group (9.86 ± 2.00 MPa). Control group underwent 100% adhesive failures. Experimental groups had predominantly mixed/cohesive failures.
Both universal adhesives increased the bond strength at resin-zirconia junction. Tetric N-Bond Universal exhibited the highest strength.
全瓷修复体的成功取决于其粘结过程。将氧化锆等晶体材料粘结到下层基底具有挑战性。最近,通用粘结剂已被开发出来。它们声称由于存在如10 - 甲基丙烯酰氧基癸基磷酸二氢酯等化合物,能够与氧化锆发生化学粘结。但对于这些粘结剂中的大多数,很少有研究证明其有效性。
本研究旨在评估两种通用粘结剂,即单涂层7通用粘结剂和Tetric N - 通用粘结剂对氧化锆 - 树脂结合处剪切粘结强度的影响。
30个计算机辅助设计与制造(CAD - CAM)铣削的氧化锆圆柱体(5毫米×8毫米)进行喷砂处理,并分为三组:A组(对照组)不做处理,而B组和C组分别用单涂层7通用粘结剂和Tetric N - 通用粘结剂进行预处理。它们通过双固化树脂粘结剂粘结到复合表面。24小时后,进行剪切粘结强度测试并分析失效模式。
采用单因素方差分析和Tukey检验进行统计分析。
单涂层7通用粘结剂(24.43±2.66兆帕)和Tetric N - 通用粘结剂(28.61±3.11兆帕)的强度均显著高于对照组(9.86±2.00兆帕)。对照组发生100%的粘结剂失效。实验组主要发生混合/内聚性失效。
两种通用粘结剂均提高了树脂 - 氧化锆结合处的粘结强度。Tetric N - 通用粘结剂表现出最高的强度。