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使用通用粘合剂的不同功能单体时氧化锆/树脂复合材料剪切粘结强度的耐久性

The Durability of Zirconia/Resin Composite Shear Bond Strength using Different Functional Monomer of Universal Adhesives.

作者信息

Klaisiri Awiruth, Krajangta Nantawan, Thamrongananskul Niyom

机构信息

Division of Restorative Dentistry, Faculty of Dentistry, Thammasat University, Pathum Thani, Thailand.

Department of Prosthodontics, Faculty of Dentistry, Chulalongkorn University, Bangkok, Thailand.

出版信息

Eur J Dent. 2022 Oct;16(4):756-760. doi: 10.1055/s-0041-1736331. Epub 2021 Dec 13.

Abstract

OBJECTIVE

This study examined the effectiveness of different functional monomers in universal adhesives on zirconia/resin composite bond strength both before and after thermocycling. Four universal adhesives (G-premio bond universal, GPU; Clearfil Tri-S bond universal, CTB; Optibond Universal, OBU; Tetric N-bond universal; TNU), one adhesive (single bond 2; SB2), and one ceramic primer (Clearfil ceramic primer plus, CCP) were used in this study.

MATERIALS AND METHODS

Zirconia discs were prepared and embedded in acrylic. Specimens were polished and sandblasted with alumina. The specimens were randomly divided into two groups (24 hours and the thermocycled), and each group was divided into six subgroups ( = 10), according to zirconia surfaces treatments: no Tx, CCP + SB2, GPU, CTB, OBU, TNU. An Ultradent mold was located on top of the treated zirconia surface. The resin composite was filled into the mold and then light-cured. A universal testing device was used to determine the shear bond strength.

STATISTICAL ANALYSIS

The data were statistically analyzed using one-way ANOVA and Tukey's test.

RESULTS

After water storage for 24 hours, the shear bond strengths were GPU > CCP + SB2 = CTB = OBU = TNU > no Tx ( < 0.05). After thermocycling, the shear bond strengths were CCP + SB2 = GPU = CTB = TNU > OBU > no Tx ( < 0.05).

CONCLUSION

The universal adhesives containing 10-MDP exhibited the best performance in the shear bond strength of the zirconia/resin composite interface both before and after thermocycling.

摘要

目的

本研究考察了通用型粘结剂中不同功能单体在热循环前后对氧化锆/树脂复合材料粘结强度的影响。本研究使用了四种通用型粘结剂(G-premio bond universal,GPU;Clearfil Tri-S bond universal,CTB;Optibond Universal,OBU;Tetric N-bond universal,TNU)、一种粘结剂(single bond 2,SB2)和一种陶瓷底漆(Clearfil ceramic primer plus,CCP)。

材料与方法

制备氧化锆圆盘并嵌入丙烯酸树脂中。对试样进行抛光并用氧化铝喷砂处理。根据氧化锆表面处理方式,将试样随机分为两组(24小时组和热循环组),每组再分为六个亚组(n = 10):未处理(no Tx)、CCP + SB2、GPU、CTB、OBU、TNU。在处理过的氧化锆表面放置一个Ultradent模具。将树脂复合材料填充到模具中,然后进行光固化。使用万能测试装置测定剪切粘结强度。

统计分析

采用单因素方差分析和Tukey检验对数据进行统计分析。

结果

储存24小时后,剪切粘结强度为GPU > CCP + SB2 = CTB = OBU = TNU > 未处理(P < 0.05)。热循环后,剪切粘结强度为CCP + SB2 = GPU = CTB = TNU > OBU > 未处理(P < 0.05)。

结论

含10 - MDP的通用型粘结剂在热循环前后氧化锆/树脂复合材料界面的剪切粘结强度方面表现出最佳性能。

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