Alhotan Abdulaziz, Elraggal Alaaeldin, Yates Julian, Haider Julfikar, Jurado Carlos Alberto, Silikas Nikolaos
Division of Dentistry, School of Medical Sciences, University of Manchester, Manchester M13 9PL, UK.
Dental Health Department, College of Applied Medical Sciences, King Saud University, Riyadh 11454, Saudi Arabia.
Polymers (Basel). 2022 Apr 8;14(8):1521. doi: 10.3390/polym14081521.
This study aimed to evaluate the colour stability of polymethyl methacrylate (PMMA) denture base reinforced with ZrO nanoparticles, E-glass fibres, and TiO nanoparticles at various concentrations over 180-day storage in Steradent™ (STD) denture cleaner or coffee (CF). A total of 130 disc-shaped specimens were fabricated at various filler concentrations and divided into four main groups to measure the colour changes. Groups Z, T, and E consisted of PMMA reinforced with ZrO nanoparticles, TiO nanoparticles, or E-glass fibre, respectively, while Group C consisted of PMMA specimens without filler served as the control group ( = 10). The three reinforced groups were further subdivided according to the filler content ( = 10) added to the PMMA (1.5%, 3.0%, 5.0%, and 7.0% wt.%). Half of the specimens were stored in STD, while the other half was stored in CF for 180 days. A Minolta Chroma Meter was used to measure the colour changes (ΔE) at 7, 30, 90 and then 180 days. The results were assessed using two-way repeated-measures analysis of variance (RM-ANOVA) along with Bonferroni post hoc tests at a ≤ 0.05 significance level. Significant different colour changes (ΔΕ) were observed between all tested groups and across different time points. TiO-reinforced PMMA in STD/CF showed the lowest colour stability, while the E-glass fibre-reinforced PMMA in STD/CF showed the highest colour stability. Furthermore, coffee appeared to have the greatest impact on the colour change in comparison to the Steradent. The results indicated that the filler type and concentration, type of solution, and length of storage all affected the colour stability of the tested specimens.
本研究旨在评估在180天的储存期内,添加不同浓度ZrO纳米颗粒、E玻璃纤维和TiO纳米颗粒的聚甲基丙烯酸甲酯(PMMA)义齿基托在Steradent™(STD)义齿清洁剂或咖啡(CF)中的颜色稳定性。共制作了130个不同填料浓度的圆盘形试样,并分为四个主要组来测量颜色变化。Z组、T组和E组分别由添加ZrO纳米颗粒、TiO纳米颗粒或E玻璃纤维增强的PMMA组成,而C组由未添加填料的PMMA试样作为对照组( = 10)。三个增强组根据添加到PMMA中的填料含量( = 10)进一步细分(1.5%、3.0%、5.0%和7.0%重量百分比)。一半的试样储存在STD中,另一半储存在CF中180天。使用Minolta色差仪在7天、30天、90天然后180天时测量颜色变化(ΔE)。结果采用双向重复测量方差分析(RM - ANOVA)以及在显著性水平≤0.05时的Bonferroni事后检验进行评估。在所有测试组和不同时间点之间观察到显著不同的颜色变化(ΔΕ)。在STD/CF中,TiO增强的PMMA显示出最低的颜色稳定性,而在STD/CF中,E玻璃纤维增强的PMMA显示出最高的颜色稳定性。此外,与Steradent相比,咖啡似乎对颜色变化的影响最大。结果表明,填料类型和浓度、溶液类型以及储存时间均会影响测试试样的颜色稳定性。