Youssef Ahmed M, El-Sayed Hoda S, El-Nagar Islam, El-Sayed Samah M
Packaging Materials Department, National Research Centre 33 El Bohouth St. (former El Tahrir St.), Dokki Giza 12622 Egypt
Dairy Science Department, National Research Centre 33 El Bohouth St. (former El Tahrir St.), Dokki Giza 12622 Egypt.
RSC Adv. 2021 Jun 28;11(37):22571-22584. doi: 10.1039/d1ra03819b. eCollection 2021 Jun 25.
In this paper we describe the preparation of a new bionanocomposite based on carboxymethyl cellulose (CMC), Arabic gum (AG) and gelatin (GL), incorporating garlic extract (GE) and TiO nanoparticles (TiO-NPs). The prepared bionanocomposites were evaluated using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), Energy Dispersive X-ray Analysis (EDX), and scanning electron microscopy (SEM), and were evaluated for their antimicrobial effect. The permeability and thermal and mechanical properties of the films were assessed. The water vapor transmission rate (WVTR), oxygen transmission rate (OTR), and mechanical, thermal and antimicrobial properties of the prepared bionanocomposite films were enhanced by the addition of GE and TiO-NPs. The effects of GE and TiO-NPs in combination incorporated into a CMC/AG/GL blend as an edible coating on the quality of fresh Nile tilapia fish fillets during refrigerated storage were evaluated. The microbiological status and weight loss of fresh Nile tilapia fish fillets were periodically tested for 21 days during storage at 4 °C. The results indicated that GE combined with TiO-NPs has a synergistic influence on the enhancement of the preservation properties of CMC/AG/GL/GE-TiO bionanocomposites for refrigerated tilapia fish fillets, which could control microbial growth, and decrease weight loss during the storage of tilapia fish fillets.
在本文中,我们描述了一种基于羧甲基纤维素(CMC)、阿拉伯胶(AG)和明胶(GL)制备的新型生物纳米复合材料,其中包含大蒜提取物(GE)和二氧化钛纳米颗粒(TiO-NPs)。使用X射线衍射(XRD)、傅里叶变换红外光谱(FTIR)、能量色散X射线分析(EDX)和扫描电子显微镜(SEM)对制备的生物纳米复合材料进行了评估,并对其抗菌效果进行了评价。评估了薄膜的渗透性、热性能和机械性能。添加GE和TiO-NPs提高了制备的生物纳米复合薄膜的水蒸气透过率(WVTR)、氧气透过率(OTR)以及机械、热和抗菌性能。评估了作为可食用涂层掺入CMC/AG/GL共混物中的GE和TiO-NPs组合对冷藏尼罗罗非鱼鱼片品质的影响。在4℃储存期间,定期测试新鲜尼罗罗非鱼鱼片的微生物状况和重量损失,为期21天。结果表明,GE与TiO-NPs结合对增强CMC/AG/GL/GE-TiO生物纳米复合材料对冷藏罗非鱼鱼片的保鲜性能具有协同作用,可控制微生物生长,并减少罗非鱼鱼片储存期间的重量损失。