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高机械处理和长期退火对TiO纳米晶体的晶体结构和热稳定性的影响。

Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of TiO nanocrystals.

作者信息

Valeeva Albina A, Nazarova Svetlana Z, Schröttner Hartmuth, Gerasimov Evgeny Yu, Rempel Andrey A

机构信息

Institute of Solid State Chemistry of the Ural Branch of the Russian Academy of Sciences 620990 Ekaterinburg Russia

Ural Federal University 620002 Ekaterinburg Russia.

出版信息

RSC Adv. 2020 Jul 7;10(43):25717-25720. doi: 10.1039/d0ra03862h. eCollection 2020 Jul 3.

DOI:10.1039/d0ra03862h
PMID:35518592
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9055306/
Abstract

The effect of high-energy milling and long-term annealing on the stability of TiO nanocrystals was studied using a magnetic susceptibility method. temperature dependences revealed that the crystal size greatly affects the magnetic susceptibility value. According to XRD, SEM and TEM data, Magnéli phases TiO, TiO, TiO and TiO are formed.

摘要

采用磁化率法研究了高能球磨和长期退火对TiO纳米晶体稳定性的影响。温度依赖性表明晶体尺寸对磁化率值有很大影响。根据XRD、SEM和TEM数据，形成了马格内利相TiO、TiO、TiO和TiO。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/dc05fd4ee64f/d0ra03862h-f5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/50ea39340a9c/d0ra03862h-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/15fd209f5fa4/d0ra03862h-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/f602ff39185f/d0ra03862h-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/53fc334485dd/d0ra03862h-f4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/dc05fd4ee64f/d0ra03862h-f5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/50ea39340a9c/d0ra03862h-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/15fd209f5fa4/d0ra03862h-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/f602ff39185f/d0ra03862h-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/53fc334485dd/d0ra03862h-f4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eed5/9055306/dc05fd4ee64f/d0ra03862h-f5.jpg

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