Yan Xintao, Xia Yuchi, He Daoguang, Lin Y C
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China.
State Key Laboratory of High Performance Complex Manufacturing, Changsha 410083, China.
Materials (Basel). 2022 Apr 27;15(9):3161. doi: 10.3390/ma15093161.
Microstructural evolution and dynamic recrystallization (DRX) behaviors of a Ni-Cr-Mo alloy were researched utilizing hot compressive experiments. The changed features of dislocation, subgrain and grain structure correlating to forming parameters were examined by transmission electron microscope (TEM) and electron backscatter diffraction (EBSD). Results illustrate that the consumption of dislocation and the coarsening of substructure/DRX grain are prominently enhanced with an increased forming temperature. However, the annihilation/interaction of dislocation and the expansion of subgrain/DRX grain boundary can be limited at a larger strain rate. Meanwhile, considering the discrepancy in DRX variation rates concerning the strain rate's ranges, an improved DRX kinetic model was developed. Compared to the classical DRX kinetic model, the good consistency between the forecasted and tested results demonstrates that the established improved DRX kinetic model can precisely characterize the DRX features of the Ni-Cr-Mo alloy over a wide strain rate range. Additionally, the EBSD's quantitative statistical results proved that the variation of DRX grain size can be supremely defined as the power formulation of the forming temperature and strain rate.
利用热压缩实验研究了一种镍铬钼合金的微观结构演变和动态再结晶(DRX)行为。通过透射电子显微镜(TEM)和电子背散射衍射(EBSD)研究了与成形参数相关的位错、亚晶粒和晶粒结构的变化特征。结果表明,随着成形温度的升高,位错的消耗以及亚结构/DRX晶粒的粗化显著增强。然而,在较大应变速率下,位错的湮灭/相互作用以及亚晶粒/DRX晶界的扩展会受到限制。同时,考虑到DRX变化率在应变速率范围内的差异,建立了改进的DRX动力学模型。与经典DRX动力学模型相比,预测结果与测试结果之间的良好一致性表明,所建立的改进DRX动力学模型能够在较宽的应变速率范围内精确地表征镍铬钼合金的DRX特征。此外,EBSD的定量统计结果证明,DRX晶粒尺寸的变化可以高度定义为成形温度和应变速率的幂函数。