Yang Qiu-Mei, Lin Yong-Cheng, Chen Ming-Song, Chen Zi-Jian
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China.
State Key Laboratory of High-Performance Complex Manufacturing, Changsha 410083, China.
Materials (Basel). 2022 Jun 6;15(11):4030. doi: 10.3390/ma15114030.
The dynamic recrystallization (DRX) features and the evolution of the microstructure of a new hot isostatic pressed (HIPed) powder metallurgy (P/M) superalloy are investigated by hot-compression tests. The sensitivity of grain dimension and DRX behavior to deformation parameters is analyzed. The results reveal that the DRX features and grain-growth behavior are significantly affected by deformation conditions. The DRX process is promoted with a raised temperature/true strain or a reduced strain rate. However, the grains grow up rapidly at relatively high temperatures. At strain rates of o.1 s and 1 s, a uniform microstructure and small grains are obtained. Due to the obvious differences in the DRX rate at various temperatures, the piecewise DRX kinetics equations are proposed to predict the DRX behavior. At the same time, a mathematical model for predicting the grain dimension and the grain growth behavior is established. To further analyze the DRX behavior and the changes in grain dimension, the hot deformation process is simulated. The developed grain-growth equation as well as the piecewise DRX kinetics equations are integrated into DEFORM software. The simulated DRX features are consistent with the test results, indicating that the proposed DRX kinetics equations and the established grain-growth model can be well used for describing the microstructure evolution. So, they are very useful for the practical hot forming of P/M superalloy parts.
通过热压缩试验研究了一种新型热等静压(HIPed)粉末冶金(P/M)高温合金的动态再结晶(DRX)特征及微观组织演变。分析了晶粒尺寸和DRX行为对变形参数的敏感性。结果表明,DRX特征和晶粒生长行为受变形条件的显著影响。提高温度/真实应变或降低应变速率可促进DRX过程。然而,在相对较高温度下晶粒会快速长大。在应变速率为0.1 s⁻¹和1 s⁻¹时,可获得均匀的微观组织和细小晶粒。由于不同温度下DRX速率存在明显差异,提出了分段DRX动力学方程来预测DRX行为。同时,建立了预测晶粒尺寸和晶粒生长行为的数学模型。为进一步分析DRX行为和晶粒尺寸变化,对热变形过程进行了模拟。将所建立的晶粒生长方程以及分段DRX动力学方程集成到DEFORM软件中。模拟的DRX特征与试验结果一致,表明所提出的DRX动力学方程和所建立的晶粒生长模型可很好地用于描述微观组织演变。因此,它们对于P/M高温合金零件的实际热成型非常有用。