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熔纺法制备YAG陶瓷纤维柔性坯体

Preparation of the Flexible Green Body of YAG Ceramic Fiber by Melt Spinning.

作者信息

Liu Hongmei, Tian Junjie, Pan Gangwei, Xie Yongjin, Yao Qing

机构信息

School of Mechanical Engineering, Nantong University, Nantong 226000, China.

School of Transportation and Civil Engineering, Nantong University, Nantong 226000, China.

出版信息

Polymers (Basel). 2022 May 20;14(10):2096. doi: 10.3390/polym14102096.

Abstract

YAG ceramic fiber, with its high thermal conductivity and easy to achieve limit size, provides design flexibility as a laser gain medium. Its mainstream forming method was mainly high-pressure extrusion, but there were disadvantages, such as lack of flexibility. In this work, the flexible green body of YAG ceramic fiber was prepared by melt spinning. The melting characteristics of TPU with four different Shore hardnesses were systematically investigated. The microstructure, element homogeneity of the surface and fracture SEM images of the prepared ceramic fiber were also analyzed in detail. The optimized process parameters of YAG ceramic fiber preparation were as follows: the melting temperature was 220 °C, the screw feed rate of the double-cone screw extruder was F = 15.0 mm/min and the TPU-95A# was used. The ceramic fiber with the mass ratio of TPU-95A# to ceramic powder = 4:6 had the best microstructure quality. It had good flexibility and could be knotted with a bending radius of about 2.5 mm, and the tensile strength reached approximately 20 MPa. These results are crucial for advancing YAG ceramic fiber applications.

摘要

YAG陶瓷纤维具有高导热性且易于达到极限尺寸,作为激光增益介质提供了设计灵活性。其主流成型方法主要是高压挤压,但存在缺乏灵活性等缺点。在本工作中,通过熔体纺丝制备了YAG陶瓷纤维的柔性坯体。系统研究了四种不同邵氏硬度的TPU的熔融特性。还详细分析了制备的陶瓷纤维的微观结构、表面元素均匀性和断裂SEM图像。YAG陶瓷纤维制备的优化工艺参数如下:熔融温度为220℃,双锥螺杆挤出机的螺杆进料速率为F = 15.0 mm/min,使用TPU-95A#。TPU-95A#与陶瓷粉末质量比为4:6的陶瓷纤维具有最佳的微观结构质量。它具有良好的柔韧性,弯曲半径约为2.5 mm时可打结,拉伸强度达到约20 MPa。这些结果对于推进YAG陶瓷纤维的应用至关重要。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b268/9147338/e40244e29cc9/polymers-14-02096-g001.jpg

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