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用于有损模式共振光纤折射仪的氮氧化硅薄膜涂层

Silicon Oxynitride Thin Film Coating to Lossy Mode Resonance Fiber-Optic Refractometer.

作者信息

Sudas Dmitriy P, Zakharov Leonid Yu, Jitov Viktor A, Golant Konstantin M

机构信息

World-Class Research Center, Peter the Great St. Petersburg Polytechnical University, Polytechnicheskaya ul. 29, 195251 St. Petersburg, Russia.

Kotel'nikov Institute of Radioengineering and Electronics, Russian Academy of Sciences, Fryazino Branch, Sq. Vvedenskogo 1, Fryazino, 141190 Moscow, Russia.

出版信息

Sensors (Basel). 2022 May 11;22(10):3665. doi: 10.3390/s22103665.

Abstract

A fiber-optic refractometer for various liquids with refractive indices in the range from 1.33 to 1.43 has been manufactured and tested. The sensor is based on a thin silicon oxynitride (SiNO) film coated thinned optic fiber section (taper) obtained in a multimode all-silica optical fiber by chemical etching of the reflective cladding. The film was deposited on the cylindrical surface of the thinned fiber by the surface plasma chemical vapor deposition method (SPCVD). Lossy mode resonance (LMR) was observed in the transmission spectrum of the coated taper at a wavelength dependent on the refractive index of the liquid in which the taper was immersed. We tested the obtained sensors in distilled water, isopropyl alcohol, dimethylformamide, and their aqueous solutions. It was found that with the help of the SPCVD, one can obtain a set of sensors in a single deposition run with the dispersion of sensitivity and spectral position of LMR no more than 5%. Maximum sensitivity of the manufactured sensors to surrounding media refractive index (SMRI) variation exceeds 1090 nm/RIU, which is the highest value recorded to date for a sensor with a non-oxide coating.

摘要

已制造并测试了一种用于折射率在1.33至1.43范围内的各种液体的光纤折射仪。该传感器基于通过对反射包层进行化学蚀刻在多模全石英光纤中获得的涂覆有薄氮氧化硅(SiNO)膜的细光纤段(锥形)。通过表面等离子体化学气相沉积法(SPCVD)将该膜沉积在细光纤的圆柱表面上。在涂覆的锥形光纤的透射光谱中观察到损耗模式共振(LMR),其波长取决于锥形光纤所浸入液体的折射率。我们在蒸馏水、异丙醇、二甲基甲酰胺及其水溶液中测试了所得传感器。结果发现,借助SPCVD,可以在单次沉积过程中获得一组传感器,其灵敏度和LMR光谱位置的分散度不超过5%。所制造的传感器对周围介质折射率(SMRI)变化的最大灵敏度超过1090 nm/RIU,这是迄今为止非氧化物涂层传感器记录的最高值。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6f80/9143494/e99f7346c7dc/sensors-22-03665-g001.jpg

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