Syrgabek Yerkanat, Alimzhanova Mereke
Center of Physical-Chemical Methods of Research and Analysis, Al-Farabi Kazakh National University, Tole bi 96a, Almaty 050012, Kazakhstan.
Faculty of Physics and Technology, Al-Farabi Kazakh National University, 71 al-Farabi Ave., Almaty 050040, Kazakhstan.
Foods. 2022 May 31;11(11):1623. doi: 10.3390/foods11111623.
Currently, research on the determination of pesticides in food products is very popular. Information obtained from research conducted so far mainly concerns the development of a methodology to determine the content of pesticides in food products. However, they do not describe the content of the pesticide used in viticulture in the resulting product. Over the past decade, this study has examined analytical methodologies for assessing pesticide residues in grapes. Scopus, Web of Science, Science Direct, PubMed, and Springer databases were searched for relevant publications. The phrases "pesticides" and "grapes" and their combinations were used to search for articles. The titles and annotations of the extracted articles have been read and studied to ensure that they meet the review criteria. The selected articles were used to compile a systematic review based on scientific research and reliable sources. The need to study the detection of pesticide residues in grapes using advanced analytical methods is confirmed by our systematic review. This review also highlights modern methods of sample preparation, such as QuEChERS, SPME, PLE, dLLME, and ADLL-ME, as well as the most used methods of separation and identification of pesticides in grapes. An overview of the countries where residual grape pesticide amounts are most studied is presented, along with the data on commonly used pesticides to control pests and diseases in grape cultivation. Finally, future possibilities and trends in the analysis of pesticide residues in grapes are discussed by various analytical methods.
目前，食品中农药测定的研究非常热门。到目前为止，从已开展的研究中获得的信息主要涉及测定食品中农药含量方法的开发。然而，它们并未描述酿酒葡萄中所使用农药在最终产品中的含量。在过去十年间，本研究对评估葡萄中农药残留的分析方法进行了考察。在Scopus、科学网、科学Direct、PubMed和施普林格数据库中搜索相关出版物。使用“农药”和“葡萄”及其组合短语来搜索文章。已阅读并研究了提取文章的标题和注释，以确保它们符合综述标准。所选文章用于基于科学研究和可靠来源编写系统综述。我们的系统综述证实了使用先进分析方法研究葡萄中农药残留检测的必要性。本综述还重点介绍了现代样品制备方法，如QuEChERS、固相微萃取、加压液体萃取、分散液液微萃取和加速分散液液微萃取，以及葡萄中农药最常用的分离和鉴定方法。介绍了对葡萄农药残留量研究最多的国家概况，以及葡萄种植中用于控制病虫害的常用农药数据。最后，通过各种分析方法讨论了葡萄中农药残留分析的未来可能性和趋势。
