Yan Zehua, Hu Jiahui, Sun Shouxue
Rongcheng College, Harbin University of Science and Technology, Weihai 264300, China.
Materials (Basel). 2024 Aug 2;17(15):3840. doi: 10.3390/ma17153840.
GH4720Li is an advanced nickel-based alloy celebrated for its remarkable high-temperature strength. This study aimed to investigate the dynamic recrystallization (DRX) behavior of novel GH4720Li superalloys microalloyed with 0.3Y via hot compression tests. A constitutive model was formulated to simulate the DRX behavior. Utilizing the stress-strain curve, the activation energy for the alloy was determined using both the Arrhenius model and the Z-parameter equation, resulting in 1117.916 kJ/mol. The microstructure evolution analysis conducted revealed that lower strain rates at elevated temperatures effectively hindered the occurrence of DRX. Conversely, the increase in the strain rate promoted DRX, producing uniform, equiaxial grains. Recrystallization calculations, along with validation experiments, demonstrated the efficacy of the Avrami model in establishing a DRX model for the alloy during hot deformation. This model accurately quantified DRX percentages under varying deformation parameters, showcasing strong agreement with the microstructure test results. The predictive capability afforded by the developed models offers valuable insights for optimizing the alloy's forging process. During the compression of the novel GH4720Li superalloy, DRX initiates when the dislocation density in a specific region surpasses a critical threshold. Concurrently, dislocation accumulation near the grain boundaries exceeds that within the grains themselves, highlighting that newly formed DRXed grains primarily emerge along the deformed grain boundaries.
GH4720Li是一种先进的镍基合金,以其卓越的高温强度而闻名。本研究旨在通过热压缩试验研究新型0.3Y微合金化GH4720Li高温合金的动态再结晶(DRX)行为。建立了一个本构模型来模拟DRX行为。利用应力-应变曲线,使用阿伦尼乌斯模型和Z参数方程确定了合金的激活能,结果为1117.916 kJ/mol。进行的微观结构演变分析表明,高温下较低的应变速率有效地阻碍了DRX的发生。相反,应变速率的增加促进了DRX,产生了均匀的等轴晶粒。再结晶计算以及验证实验证明了阿弗拉米模型在建立合金热变形过程中DRX模型方面的有效性。该模型准确地量化了不同变形参数下的DRX百分比,与微观结构测试结果显示出高度一致性。所开发模型提供的预测能力为优化合金的锻造工艺提供了有价值的见解。在新型GH4720Li高温合金的压缩过程中,当特定区域的位错密度超过临界阈值时,DRX开始。同时,晶界附近的位错积累超过了晶粒内部的位错积累,这表明新形成的DRX晶粒主要沿变形晶界出现。