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高效工程化废蛋壳-粉煤灰去除水溶液中的镉。

Highly efficient engineered waste eggshell-fly ash for cadmium removal from aqueous solution.

机构信息

Institute for Advanced Environmental Research -West University of Timisoara (ICAM -WUT), Oituz nr. 4, Timisoara, Romania.

West University of Timisoara, 4 Blvd.V.Parvan, 300223, Timisoara, Romania.

出版信息

Sci Rep. 2022 Jun 11;12(1):9676. doi: 10.1038/s41598-022-13664-6.

DOI:10.1038/s41598-022-13664-6
PMID:35690618
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9188607/
Abstract

Sustainable waste and water management are key components of the newest EU policy regarding the circular economy. Simple, performant and inexpensive water treatment methods based on reusing waste are prerequisites for human health, sustainable development and environmental remediation. The design of performant, cost-effective absorbents represents a topical issue in wastewater treatment. This study aimed to investigate the development of a newly engineered adsorbent by functionalizing two different types of waste (industrial and food) with magnetic nanoparticles as environmentally friendly, highly efficient, cheap material for cadmium removal from aqueous solutions. This nano-engineered adsorbent (EFM) derived from waste eggshell and fly ash was used to remove the cadmium from the aqueous solution. SEM analysis has demonstrated that magnetite nanoparticles were successfully loaded with each waste. In addition, was obtained a double functionalization of the eggshell particles with ash and magnetite particles. As a result of this, the EFM surface area substantially increased, as confirmed by BET. A comprehensive characterization (BET, FT-IR, SEM, XRD and TGA) was performed to study the properties of this newly engineered adsorbent. Batch experiments were conducted to investigate the influence of different reaction parameters: temperature, pH, contact time, dosage adsorbent, initial concentration. Results showed that cadmium adsorption reached equilibrium in 120 min., at pH 6.5, for 0.25 g of adsorbent. The maximum efficiency was 99.9%. The adsorption isotherms research displayed that the Cd adsorption fitted on the Freundlich model indicated a multi-molecular layer adsorption process. In addition, the thermodynamic study (ΔG < 0, ΔH > 0; ΔS > 0) shows that cadmium adsorption is a spontaneous and endothermic process. The adsorbent kinetic study was described with the pseudo-second-order model indicating a chemisorption mechanism. Desorption results showed that the nano-engineered adsorbent (EFM) can be reused. These data confirmed the possibility to enrich relevant theoretical knowledge in the field of waste recovery for obtaining newly designed adsorbents, performant and inexpensive for wastewater remediation.

摘要

可持续的废物和水资源管理是欧盟最新循环经济政策的关键组成部分。基于废物再利用的简单、高效和廉价的水处理方法是人类健康、可持续发展和环境修复的前提。设计高效、经济实惠的吸附剂是废水处理中的一个热门问题。本研究旨在通过用磁性纳米粒子对两种不同类型的废物（工业废物和食品废物）进行功能化，开发一种新型的吸附剂，这种纳米粒子是一种环保、高效、廉价的从水溶液中去除镉的材料。这种由废蛋壳和粉煤灰衍生的纳米工程吸附剂（EFM）用于从水溶液中去除镉。SEM 分析表明，成功地在每种废物上负载了磁铁矿纳米粒子。此外，还实现了蛋壳颗粒与粉煤灰和磁铁矿颗粒的双重功能化。结果，EFM 的表面积大大增加，这一点通过 BET 得到了证实。对这种新型吸附剂进行了全面的特性分析（BET、FT-IR、SEM、XRD 和 TGA）。进行了批量实验，以研究不同反应参数（温度、pH 值、接触时间、吸附剂用量、初始浓度）的影响。结果表明，镉吸附在 120 分钟内达到平衡，在 pH 值为 6.5、吸附剂用量为 0.25 克时，达到 99.9%的最大效率。吸附等温线研究表明，Cd 吸附符合 Freundlich 模型，表明这是一个多分子层吸附过程。此外，热力学研究（ΔG<0、ΔH>0；ΔS>0）表明，镉吸附是一个自发的吸热过程。吸附剂动力学研究用准二级模型来描述，表明这是一个化学吸附机制。解吸结果表明，纳米工程吸附剂（EFM）可以重复使用。这些数据证实了在废物回收领域获得新型设计的吸附剂的相关理论知识的丰富，这些吸附剂高效且廉价，可用于废水修复。

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5
The selective adsorption performance and mechanism of multiwall magnetic carbon nanotubes for heavy metals in wastewater.多壁磁碳纳米管对废水中重金属的选择性吸附性能及机理。
Sci Rep. 2021 Aug 19;11(1):16878. doi: 10.1038/s41598-021-96465-7.
6
Magnetically tuning microwave propagation parameters in ferrofluids.铁磁流体中微波传播参数的磁调谐
Eur Phys J E Soft Matter. 2021 Jun 22;44(6):83. doi: 10.1140/epje/s10189-021-00087-w.
7
Cadmium toxicity in plants: Impacts and remediation strategies.植物中的镉毒性：影响与修复策略。
Ecotoxicol Environ Saf. 2021 Mar 15;211:111887. doi: 10.1016/j.ecoenv.2020.111887. Epub 2021 Jan 12.
8
The Effects of Cadmium Toxicity.镉毒性的影响。
Int J Environ Res Public Health. 2020 May 26;17(11):3782. doi: 10.3390/ijerph17113782.
9
Adsorption kinetic models: Physical meanings, applications, and solving methods.吸附动力学模型：物理意义、应用和求解方法。
J Hazard Mater. 2020 May 15;390:122156. doi: 10.1016/j.jhazmat.2020.122156. Epub 2020 Jan 25.
10
Adsorption of Cadmium Ions from an Aqueous Solution on a Highly Stable Dopamine-Modified Magnetic Nano-Adsorbent.水溶液中镉离子在高度稳定的多巴胺修饰磁性纳米吸附剂上的吸附
Nanoscale Res Lett. 2019 Nov 28;14(1):352. doi: 10.1186/s11671-019-3154-0.