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辅料壁材对姜辣素油树脂微胶囊形成的影响:评估其物理化学、抗氧化和结构性能。

Effect of excipient wall materials on the development of ginger oleoresin microcapsules: assessing the physicochemical, antioxidant and structural properties.

机构信息

Department of Food Technology, University of Kashmir, Srinagar, India.

出版信息

J Sci Food Agric. 2023 Jan 15;103(1):73-82. doi: 10.1002/jsfa.12113. Epub 2022 Aug 12.

Abstract

BACKGROUND

Ginger oleoresin is prone to destruction from air, light and high temperatures and has a limited shelf life if kept improperly. Its viscous and sticky characteristics also make it difficult to handle and utilize. These issues can be solved via microencapsulation. The goal of this research was to evaluate how different wall materials affect the properties of microencapsulated ginger oleoresin powder.

RESULTS

Ginger oleoresin microcapsules were developed through spray drying technique using gum acacia (GA) and whey protein isolate (WPI) as wall materials. The characteristics of the obtained powder, including water activity, wettability and encapsulation efficiency, were evaluated, corresponded to values of 0.20, 90.54 s and 84.15% for whey protein isolate-based ginger oleoresin powder. Whey protein isolate microcapsules also exhibited higher phenolic content (27.26 mg gallic acid equivalents g ), total flavonoid (2.94 mg quercetin equivalents g ) and 2,2-diphenyl-1-picrylhydrazyl radical scavenging activity (68.71%) than GA microcapsules. Both WPI- and GA-based oleoresin microcapsules displayed poor flowability, but possessed a metastable amorphous state as indicated by X-ray diffraction. GA-encapsulated oleoresin microcapsules showed a significant increase in particle size (1983 nm) compared to WPI oleoresin microcapsules. Fourier transform infrared analysis of the developed oleoresin microcapsules indicated no change in molecular structure except for a variation in peak intensity.

CONCLUSION

Whey protein isolate proved to be more efficient in maintaining the physicochemical and antioxidant activity of spray-dried ginger oleoresin powder. The present study revealed whey protein-based oleoresin powder could be used as a therapeutic agent in various nutraceutical applications. © 2022 Society of Chemical Industry.

摘要

背景

姜油树脂容易受到空气、光照和高温的破坏,如果储存不当,其保质期有限。其粘性和粘性特点也使其难以处理和利用。这些问题可以通过微胶囊化来解决。本研究的目的是评估不同壁材如何影响微胶囊化姜油树脂粉末的性质。

结果

通过喷雾干燥技术用阿拉伯胶(GA)和乳清蛋白分离物(WPI)作为壁材开发了姜油树脂微胶囊。对所得粉末的特性,包括水活度、润湿性和包埋效率进行了评估,与乳清蛋白分离物基姜油树脂粉末的值 0.20、90.54 s 和 84.15%相对应。乳清蛋白分离物微胶囊还表现出更高的酚含量(27.26 mg 没食子酸当量 g)、总黄酮(2.94 mg 槲皮素当量 g)和 2,2-二苯基-1-苦基肼自由基清除活性(68.71%)比 GA 微胶囊高。基于 WPI 和 GA 的油树脂微胶囊均表现出较差的流动性,但 X 射线衍射表明它们处于亚稳非晶态。与 WPI 油树脂微胶囊相比,GA 包封的油树脂微胶囊的粒径(1983 nm)显著增加。对所开发的油树脂微胶囊的傅里叶变换红外分析表明,除了峰强度的变化外,分子结构没有变化。

结论

乳清蛋白分离物在保持喷雾干燥姜油树脂粉末的物理化学和抗氧化活性方面更为有效。本研究表明,基于乳清蛋白的油树脂粉末可用于各种营养应用的治疗剂。© 2022 化学工业协会。

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