Azmy Emad, Al-Kholy Mohamed Reda Zaki, Fattouh Mohamed, Kenawi Laila Mohamed Mohamed, Helal Mohamed Ahmed
Elmarg Students' Clinic, General Authority of Health Insurance, Western Elmarg Area, Cairo, Egypt.
Department of Removable Prosthodontics, Faculty of Dental Medicine, Al-Azhar University, Cairo, Egypt.
Int J Biomater. 2022 Jul 5;2022:1165431. doi: 10.1155/2022/1165431. eCollection 2022.
This study aimed to evaluate the effect of nanoparticles, zirconium dioxide (ZrO), titanium dioxide (TiO), and silicon dioxide (SiO), on flexural strength (FS), hardness, and wear resistance of light cured dental composite resin.
210 rectangular and disc-shaped composite resin specimens were fabricated with dimensions (25 × 2 × 2 ± 0.03 mm) and (6×4 ± 0.03 mm) for FS, hardness, and wear resistance, respectively (70/test). Specimens of each test were divided according to nanofillers into four groups, unmodified as control, ZrO (Z), TiO (T), and SiO (S) groups; each one was further subdivided into two subgroups according to nanoparticles concentration, 3wt.% and 7wt.% (Z3, Z7, T3, T7, S3, and S7), 10 specimens of each subgroup. A3-point bending test and Vickers hardness test were used for FS and hardness measurements, respectively. Wear resistance was evaluated by the differences in surface roughness of tested specimens before and after wear test. Two-way and 1-way ANOVA and Bonferroni's post hoc tests were done for data analysis ( = 0.05).
Two-way ANOVA for FS and wear resistance showed that there was a significant interaction between type of nanoparticles and concentration of nanoparticles ( < 0.001) while two-way ANOVA for hardness showed that both type of nanoparticles and concentration of nanoparticles had a significant effect ( < 0.001), while the effect of their interaction was not statistically significant (=0.142). 1-way-ANOVA test showed significant increase in FS and wear resistance for all tested groups ( < 0.001 and < 0.001, respectively) except T7 and S7. Also, there was a significant enhancement in hardness for all tested groups ( < 0.001).
Modification of light cured composite resin with certain amounts of nanoparticles (3% and 7% of ZrO and 3% of TiO and SiO) can be beneficial in improving flexural strength and wear resistance while hardness of composite resin was increased with all NPs additions.
本研究旨在评估纳米颗粒二氧化锆(ZrO)、二氧化钛(TiO)和二氧化硅(SiO)对光固化牙科复合树脂的弯曲强度(FS)、硬度和耐磨性的影响。
制备了210个矩形和圆盘形复合树脂试样,尺寸分别为(25×2×2±0.03mm)和(6×4±0.03mm),分别用于测试FS、硬度和耐磨性(每组70个)。每个测试的试样根据纳米填料分为四组,未改性的作为对照组,ZrO(Z)、TiO(T)和SiO(S)组;每组再根据纳米颗粒浓度进一步细分为两个亚组,3wt.%和7wt.%(Z3、Z7、T3、T7、S3和S7),每个亚组10个试样。分别采用三点弯曲试验和维氏硬度试验测量FS和硬度。通过磨损试验前后测试试样表面粗糙度之差评估耐磨性。采用双向和单向方差分析以及Bonferroni事后检验进行数据分析(α=0.05)。
FS和耐磨性的双向方差分析表明,纳米颗粒类型与纳米颗粒浓度之间存在显著交互作用(P<0.001),而硬度的双向方差分析表明,纳米颗粒类型和纳米颗粒浓度均有显著影响(P<0.001),但其交互作用的影响无统计学意义(P=0.142)。单向方差分析测试表明,除T7和S7外,所有测试组的FS和耐磨性均显著增加(分别为P<0.001和P<0.001)。此外,所有测试组的硬度均有显著提高(P<0.001)。
用一定量的纳米颗粒(3%和7%的ZrO以及3%的TiO和SiO)改性光固化复合树脂有利于提高弯曲强度和耐磨性,同时添加所有纳米颗粒均可提高复合树脂硬度。