Chiapinotto Gratcheva Falcão, da Rosa Lucas Saldanha, Scotti Nicola, Kleverlaan Cornelis Johannes, Valandro Luiz Felipe, Pereira Gabriel Kalil Rocha
Graduate Program in Dentistry, Faculty of Dentistry, Federal University of Santa Maria (UFSM), Santa Maria, Rio Grande do Sul State, Brazil.
MSciD and PhD Post-Graduate Program in Oral Science, Faculty of Dentistry, Federal University of Santa Maria (UFSM), Santa Maria, Rio Grande do Sul State, Brazil.
J Mech Behav Biomed Mater. 2022 Oct;134:105373. doi: 10.1016/j.jmbbm.2022.105373. Epub 2022 Jul 19.
The present study aimed to determine the influence of adhesive luting on the fatigue mechanical properties of simplified lithium disilicate crowns luted to dentin analogues preparations, and to compare two different approaches of simulation of a non-adhesive luting procedure. To this end, 30 prosthetic preparations of glass fiber-filled epoxy resin used as dentin analogues were milled and lithium disilicate crowns were pressed (1.5 mm thickness), which were allocated into three different groups: resin cement (RC), resin cement isolated by paraffin oil (RCI) and zinc phosphate cement (ZP). For luting procedures, the ceramic crowns of the RC and RCI groups had their internal surface treated with 5% hydrofluoric acid and universal primer. Afterwards, a thin layer of paraffin oil was applied onto the ceramic crown intaglio surface in the RCI group. The dentin analogues were treated with 10% hydrofluoric acid, followed by primer application and luting as recommended by the manufacturer. No previous surface treatments were performed for the ZP group, and the cement was applied as recommended. The fatigue test was run under cyclic fatigue (load 400-2000 N, step-size 100 N, 15,000 cycles/step, frequency 20 Hz) until failure detection (radial crack) by transillumination. The fatigue failure load (FFL), number of cycles until failure (CFF), and survival rate in each testing step were recorded. The RC group presented a higher FFL, CFF and survival rate compared to the other groups (p < 0.001), which were statistically equal to each other (p > 0.05). Weibull analysis detected no difference between groups for the Weibull module. Therefore, loss of adhesion between the evaluated substrates induces a significant reduction in load-bearing capacity under fatigue of the lithium disilicate crowns, strengthening the strong-importance of long-lasting adhesion for crown's survival. In addition, different methods for the simulation of non-adhesive conditions induce the same performance in the explored outcomes, confirming that both are valid approaches for laboratory studies.
本研究旨在确定粘结固位对粘结于牙本质类似物预备体上的简化二硅酸锂全冠疲劳力学性能的影响,并比较模拟非粘结固位程序的两种不同方法。为此,制备了30个用作牙本质类似物的玻璃纤维增强环氧树脂修复体预备体,铣削后压制二硅酸锂全冠(厚度1.5毫米),并将其分为三个不同组:树脂水门汀(RC)组、用石蜡油隔离的树脂水门汀(RCI)组和磷酸锌水门汀(ZP)组。对于固位程序,RC组和RCI组的陶瓷全冠内表面用5%氢氟酸和通用底漆处理。之后,在RCI组的陶瓷全冠凹面表面涂一层薄石蜡油。牙本质类似物用10%氢氟酸处理,然后按制造商建议涂底漆并进行固位。ZP组之前未进行表面处理,按建议应用水门汀。在循环疲劳(载荷400 - 2000 N,步长100 N,每步15000次循环,频率20 Hz)下进行疲劳试验,直至通过透照检测到失效(径向裂纹)。记录每个测试步骤的疲劳失效载荷(FFL)、直至失效的循环次数(CFF)和生存率。与其他组相比,RC组呈现出更高的FFL、CFF和生存率(p < 0.001),其他组之间在统计学上无差异(p > 0.05)。威布尔分析未检测到各组之间威布尔模量的差异。因此,所评估的基底之间粘结力的丧失会导致二硅酸锂全冠在疲劳状态下的承载能力显著降低,这强化了持久粘结对全冠留存的重要性。此外,模拟非粘结条件的不同方法在探索的结果中表现出相同的性能,证实这两种方法都是实验室研究的有效方法。