MSciD and PhD Post-Graduate Program in Oral Sciences, Federal University of Santa Maria (UFSM), Santa Maria, RS, Brazil.
Academic Centre for Dentistry Amsterdam (ACTA), Department of Oral Regenerative Medicine, University of Amsterdam and Vrije Universiteit Amsterdam, 1081 LA, Amsterdam, the Netherlands.
J Mech Behav Biomed Mater. 2023 Feb;138:105604. doi: 10.1016/j.jmbbm.2022.105604. Epub 2022 Dec 5.
To evaluate the fatigue behavior of lithium disilicate crowns with a simplified anatomy against progressive cement/ceramic debonding scenarios.
Lithium disilicate crowns were fabricated via CAD/CAM and luted onto a dentin analogue material using resin cement following the manufacturer's instructions. Then, the different crown regions were isolated with paraffin oil for the absence of chemical adhesion according to four experimental groups (n = 15): Shoulder; Shoulder + Axial; Fully isolated; and Control (no insulation/fully bonded). Load to failure tests (n = 3) were run to determine cyclic fatigue parameters, and the specimens were subsequently submitted to a cyclic fatigue test (n = 12) (initial load 200 N for 5000 cycles, step 100 N, 15,000 cycles/step, frequency 20 Hz) until cracks were observed, and later fracture. The data were analyzed by Kaplan-Meier + Mantel-Cox post-hoc tests for both outcomes (cracks and fracture). Fractographic, cross-sectional surface, and finite element (FEA) analyzes were performed.
When it comes to crack occurrence when the chemical adhesion to the occlusal surface is compromised, there is worsening (p < 0.05) in fatigue behavior compared to groups where the occlusal portion of the crown is still bonded. Considering fracture occurrence, there was no difference (p > 0.05) among the tested groups. All cracks occurred in the occlusal portion, first as a radial crack at the ceramic intaglio surface, and posteriorly unleashing a Hertzian cone crack at the top surface, resulting in fractures on the frontal walls. The interface analysis showed no interference of the insulating agent. FEA showed that as the isolated areas increased, there was also an increase in both tensile and shear stresses concentration in the crown and in the cement layer.
The chemical adhesion between cement and ceramic is essential for better fatigue behavior of lithium disilicate crowns with a simplified anatomy, especially in the occlusal portion, but the restoration performance is impaired when such adhesion is compromised. There is an increase in crown and cement stress concentration with the progressive loss of chemical bonding of the crown's walls.
评估简化解剖结构的二硅酸锂瓷全冠在渐进性的粘结/陶瓷脱粘情况下的疲劳性能。
通过 CAD/CAM 制作二硅酸锂瓷全冠,并按照制造商的说明使用树脂水门汀粘结到牙本质模拟材料上。然后,根据四个实验组(n=15),用石蜡油隔离不同的冠部区域,以防止化学粘结:肩台;肩台+轴面;完全隔离;对照组(无隔离/完全粘结)。进行失效负载测试(n=3)以确定循环疲劳参数,然后将试件进行循环疲劳测试(n=12)(初始负载 200 N 5000 次循环,每次增加 100 N,15000 次循环/步,频率 20 Hz),直到观察到裂纹,然后发生断裂。使用 Kaplan-Meier+Mantel-Cox 事后检验分析两种结果(裂纹和断裂)的数据。进行了断口形貌、横截面表面和有限元(FEA)分析。
当考虑到牙合面化学粘结被破坏时,发生裂纹的情况与牙合面部分仍粘结的组相比,疲劳性能恶化(p<0.05)。考虑到发生断裂的情况,各实验组之间没有差异(p>0.05)。所有的裂纹都发生在牙合面部分,首先是陶瓷凹面表面的放射状裂纹,随后在顶表面释放出赫兹锥形裂纹,导致前壁断裂。界面分析显示隔离剂没有干扰。FEA 显示,随着隔离区域的增加,牙冠和粘结层中的拉伸和剪切应力集中也随之增加。
对于简化解剖结构的二硅酸锂瓷全冠,粘结剂与陶瓷之间的化学粘结对于更好的疲劳性能至关重要,特别是在牙合面部分,但当这种粘结被破坏时,修复性能会受到影响。随着牙冠壁化学粘结的逐渐丧失,牙冠和粘结层的应力集中增加。