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利用气相色谱-离子迁移谱联用、香气提取稀释分析、香气重组和排除研究法对鲢鱼鱼糜凝胶中回热风味化合物的特征进行研究。

Characterization of Warmed-Over Flavor Compounds in Surimi Gel Made from Silver Carp () by Gas Chromatography-Ion Mobility Spectrometry, Aroma Extract Dilution Analysis, Aroma Recombination, and Omission Studies.

机构信息

Engineering Research Center of Green development for Conventional Aquatic Biological Industry in the Yangtze River Economic Belt, Ministry of Education, Wuhan, Hubei Province 430070, P. R. China.

College of Fisheries, Huazhong Agricultural University, Wuhan, Hubei Province 430070, P. R. China.

出版信息

J Agric Food Chem. 2022 Aug 3;70(30):9451-9462. doi: 10.1021/acs.jafc.2c02119. Epub 2022 Jul 25.

Abstract

The warmed-over flavor (WOF) in surimi gels was characterized by gas chromatography-ion mobility spectrometry, aroma extract dilution analysis, aroma recombination, and omission studies. Surimi gels with different WOF levels were prepared by different gelling temperatures, and surimi gels heated at 90, 100, and 121 °C were considered as the samples with light, strong, and medium WOF, respectively. Based on the quantification and odor activity values, 14 aldehydes, 2 ketones, 3 alcohols, 2 benzene-containing compounds, 2 N-containing compounds, 3 S-containing compounds, 3 lactones, undecanoic acid, and 4-methylphenol were recombined to build a spiked model for surimi gels with the strongest WOF, which showed the highest similarity with the original sample. Finally, a triangle test involving omission of the aroma compounds from the spiked model proved that the WOF in surimi gels was attributed to (,)-2,4-decadienal, heptanal, octanal, nonanal, decanal, ()-2-nonenal, ()-2-octenal, ()-2-decenal, (,)-2,4-heptadienal, 2,3-pentanedione, 2,6-dimethylpyrazine, 2-propylpyridine, benzothiazole, 2-methoxybenzenethiol, and 2-furfurylthiol.

摘要

加热后风味(WOF)在鱼糜凝胶中的特征采用气相色谱-离子淌度谱、香气提取稀释分析、香气重组和排除研究进行了描述。通过不同的凝胶温度制备具有不同 WOF 水平的鱼糜凝胶,将在 90、100 和 121°C 加热的鱼糜凝胶分别视为具有轻、强和中 WOF 的样品。基于定量和气味活性值,14 种醛类、2 种酮类、3 种醇类、2 种含苯化合物、2 种含氮化合物、3 种含硫化合物、3 种内酯、十一烷酸和 4-甲基苯酚被重组为具有最强 WOF 的鱼糜凝胶的加标模型,该模型与原始样品具有最高的相似度。最后,一项涉及从加标模型中排除香气化合物的三角测试证明,鱼糜凝胶中的 WOF 归因于(,)-2,4-癸二烯醛、庚醛、辛醛、壬醛、癸醛、()-2-壬烯醛、()-2-辛烯醛、()-2-癸烯醛、(,)-2,4-庚二烯醛、2,3-戊二酮、2,6-二甲基吡嗪、2-丙基吡啶、苯并噻唑、2-甲氧基苯硫酚和 2-糠基硫醇。

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