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低压等离子体处理羊毛织物对其用聚（3,4-乙撑二氧噻吩）：聚苯乙烯磺酸盐进行染色的影响。

Impact of Low-Pressure Plasma Treatment of Wool Fabric for Dyeing with PEDOT: PSS.

作者信息

Petkevičiūtė Julija, Sankauskaitė Audronė, Jasulaitienė Vitalija, Varnaitė-Žuravliova Sandra, Abraitienė Aušra

机构信息

Center for Physical Sciences and Technology, Department of Textiles Technology, Demokratu˛ Str. 53, LT-48485 Kaunas, Lithuania.

Center for Physical Sciences and Technology, Department of Characterisation of Materials Structure, Saulėtekio al. 3, LT-10257 Vilnius, Lithuania.

出版信息

Materials (Basel). 2022 Jul 8;15(14):4797. doi: 10.3390/ma15144797.

DOI:10.3390/ma15144797
PMID:35888265
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9321670/
Abstract

This study presents the effect of non-thermal plasma modification on the changes of surface morphology, color characteristics and electrical conductivity of wool fabric dyed with intrinsically conductive polymer (ICP) poly (3,4-ethylenedioxythiophene) polystyrene sulfonate (PEDOT: PSS). The wool fabric was treated with an aqueous dispersion of PEDOT: PSS, Clevios F ET, providing electrically conductive properties to textiles. The wool fabric, containing basic groups of amines (NH), was pre-activated with low-pressure plasma of non-polymer forming nitrogen (N) gas before exhaust dyeing with PEDOT: PSS at 90 °C was applied. This treatment imparted hydrophilicity, reduced felting, increased adhesion, improved dye ability and ensured that more PEDOT: PSS negatively charged sulfonate (-SO3-) counter ions would be electrostatically bounded with the cationic protonated amine groups of the wool fiber. Initially, before (N) plasma treatment and after fabrics were evaluated according to the test method for aqueous liquid repellency, the surface morphology of the plasma-modified and -unmodified wool dyed fabric was observed with scanning electron microscopy (SEM). The functional groups introduced onto the surface after N gas plasma treatment of wool fabric were characterized by X-ray photoelectron and FTIR-ATR spectroscopy. The results of color difference measurements show that N gas plasma treatments provide more intense color on Clevios F ET dyed wool fabric and retain its electrical conductivity.

摘要

本研究呈现了非热等离子体改性对用本征导电聚合物（ICP）聚（3,4 - 乙撑二氧噻吩）聚苯乙烯磺酸盐（PEDOT:PSS）染色的羊毛织物表面形态、颜色特征和电导率变化的影响。羊毛织物用PEDOT:PSS的水分散体Clevios F ET进行处理，赋予纺织品导电性能。在90℃用PEDOT:PSS进行浸染之前，含有胺基（NH）碱性基团的羊毛织物先用非聚合形成的氮气（N）的低压等离子体进行预活化。这种处理赋予了亲水性，减少了毡缩，增加了附着力，提高了染色能力，并确保更多带负电荷的PEDOT:PSS磺酸根（-SO3-）抗衡离子会与羊毛纤维的阳离子质子化胺基静电结合。最初，在（N）等离子体处理之前和之后，根据水性液体拒水测试方法对织物进行评估，用扫描电子显微镜（SEM）观察了经等离子体改性和未改性的羊毛染色织物的表面形态。通过X射线光电子能谱和傅里叶变换红外衰减全反射光谱（FTIR - ATR）对羊毛织物经氮气等离子体处理后引入到表面的官能团进行了表征。色差测量结果表明，氮气等离子体处理使Clevios F ET染色的羊毛织物颜色更鲜艳，并保持其电导率。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a648/9321670/43b73be67621/materials-15-04797-g014.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a648/9321670/60b750175a8f/materials-15-04797-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a648/9321670/24b9b87148a6/materials-15-04797-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a648/9321670/61890946c80e/materials-15-04797-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a648/9321670/2f99a4222430/materials-15-04797-g011.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a648/9321670/43b73be67621/materials-15-04797-g014.jpg

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