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湿热老化过程中影响环氧基材料水分扩散的参数——基于统计分析的综述

Parameters Influencing Moisture Diffusion in Epoxy-Based Materials during Hygrothermal Ageing-A Review by Statistical Analysis.

作者信息

Gillet Camille, Tamssaouet Ferhat, Hassoune-Rhabbour Bouchra, Tchalla Tatiana, Nassiet Valérie

机构信息

Laboratoire Génie de Production, INP-ENIT, Université de Toulouse, 47 Av. d'Azereix, 65000 Tarbes, France.

Safran Aircraft Engines, site de Villaroche, 77550 Moissy-Cramayel, France.

出版信息

Polymers (Basel). 2022 Jul 12;14(14):2832. doi: 10.3390/polym14142832.

Abstract

The hygrothermal ageing of epoxy resins and epoxy matrix composite materials has been studied many times in the literature. Models have been developed to represent the diffusion behaviour of the materials. For reversible diffusions, Fick, Dual-Fick and Carter and Kibler models are widely used. Many parameters, correlated or not, have been identified. The objectives of this review by statistical analysis are to confirm or infirm these correlations, to highlight other correlations if they exist, and to establish which are the most important to study. This study focuses on the parameters of the Fick, Dual-Fick and Carter and Kibler models. For this purpose, statistical analyses are performed on data extracted and calculated from individuals described in the literature. Box plot and PCA analyses were chosen. Differences are then noticeable according to the different qualitative parameters chosen in the study. Moreover, correlations, already observed in the literature for quantitative variables, are confirmed. On the other hand, differences appear which may suggest that the models used are inappropriate for certain materials.

摘要

环氧树脂及环氧基复合材料的湿热老化在文献中已被多次研究。已开发出模型来描述材料的扩散行为。对于可逆扩散,菲克模型、双菲克模型以及卡特和基布勒模型被广泛使用。已识别出许多参数,这些参数有的相关,有的不相关。本综述通过统计分析的目的是确认或否定这些相关性,若存在其他相关性则予以突出,并确定哪些是最值得研究的。本研究聚焦于菲克模型、双菲克模型以及卡特和基布勒模型的参数。为此,对从文献中描述的个体提取和计算的数据进行了统计分析。选择了箱线图分析和主成分分析。根据研究中选择的不同定性参数,差异随后变得明显。此外,文献中已观察到的定量变量之间的相关性得到了确认。另一方面,出现的差异可能表明所使用的模型不适用于某些材料。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/b20c/9325284/f192c530adcd/polymers-14-02832-g001.jpg

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